Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis-

Base Information

• Chemical Name: Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis-
• CAS No.: 32497-38-4
• Molecular Formula: C32H20 N2 O6
• Molecular Weight: 528.521
• European Community (EC) Number: 251-066-4
• DSSTox Substance ID: DTXSID5067689
• Mol file: 32497-38-4.mol

Synonyms:32497-38-4;EINECS 251-066-4;Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis-;Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo(1,1'-bianthracene)-2,2'-diyl)bis-;N,N'-(9,9',10,10'-Tetrahydro-9,9',10',10'-tetraoxo(1,1'-bianthracene)-2,2'-diyl)bisacetamide;N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bisacetamide;DTXSID5067689;C32-H20-N2-O6;W-110819;N,N'-(9,9',10,10'-Tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis(acetamide)

Chemical Property of Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis-

Chemical Property:

• Boiling Point: 870.2°Cat760mmHg
• Flash Point: 269.5°C
• PSA: 133.46000
• Density: 1.467g/cm³
• LogP: 6.12020
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 528.13213636
• Heavy Atom Count: 40
• Complexity: 1030

Purity/Quality:

99% ^*data from raw suppliers

N,N'-(9,9',10,10'-TETRAHYDRO-9,9',10',10'-TETRA-OXO-[1,1'-BIANTHRACENE]-2,2'-DIYL)-BIS-ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=C(C2=C(C=C1)C(=O)C3=CC=CC=C3C2=O)C4=C(C=CC5=C4C(=O)C6=CC=CC=C6C5=O)NC(=O)C

Technology Process of Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis-

There total 3 articles about Acetamide, N,N'-(9,9',10,10'-tetrahydro-9,9',10',10'-tetraoxo[1,1'-bianthracene]-2,2'-diyl)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-(1-bromoanthraquinon-2-yl)acetamide → N,N’-(1,1’-bianthracene-9,9’,10,10’-tetraon-2,2’-diyl)diacetamide (32497-38-4)

Guidance literature:

With iodine; In N,N-dimethyl-formamide; at 110 ℃; for 4h; Inert atmosphere;

DOI:10.1002/chem.201600513

Reference yield:

2-aminoanthraquinone (117-79-3) → N,N’-(1,1’-bianthracene-9,9’,10,10’-tetraon-2,2’-diyl)diacetamide (32497-38-4)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: toluene / 20 h / Reflux; Inert atmosphere

3: iodine / N,N-dimethyl-formamide / 4 h / 110 °C / Inert atmosphere

With N-Bromosuccinimide; iodine; In N,N-dimethyl-formamide; toluene; 3: |Ullmann Condensation;

DOI:10.1002/chem.201600513

Reference yield:

→ N,N’-(1,1’-bianthracene-9,9’,10,10’-tetraon-2,2’-diyl)diacetamide (32497-38-4)

Guidance literature:

aus 1-Chlor-2-amino-anthrachinon, 1) Acetanhydrid, 2) Cu;

upstream raw materials:

2-aminoanthraquinone

Downstream raw materials:

flavanthrone