Propanoic acid, 3-[3-hydroxy-2-(hydroxymethyl)-2-methyl-1-oxopropoxy]-2-[[3-hydroxy-2- (hydroxymethyl)-2-methyl-1-oxopropoxy]methyl]-2-methyl-, phenylmethyl ester

Base Information

• Chemical Name: Propanoic acid, 3-[3-hydroxy-2-(hydroxymethyl)-2-methyl-1-oxopropoxy]-2-[[3-hydroxy-2- (hydroxymethyl)-2-methyl-1-oxopropoxy]methyl]-2-methyl-, phenylmethyl ester
• CAS No.: 199457-34-6
• Molecular Formula: C22H32O10
• Molecular Weight: 456.49

Synonyms:

Chemical Property of Propanoic acid, 3-[3-hydroxy-2-(hydroxymethyl)-2-methyl-1-oxopropoxy]-2-[[3-hydroxy-2- (hydroxymethyl)-2-methyl-1-oxopropoxy]methyl]-2-methyl-, phenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Propanoic acid, 3-[3-hydroxy-2-(hydroxymethyl)-2-methyl-1-oxopropoxy]-2-[[3-hydroxy-2- (hydroxymethyl)-2-methyl-1-oxopropoxy]methyl]-2-methyl-, phenylmethyl ester

There total 4 articles about Propanoic acid, 3-[3-hydroxy-2-(hydroxymethyl)-2-methyl-1-oxopropoxy]-2-[[3-hydroxy-2- (hydroxymethyl)-2-methyl-1-oxopropoxy]methyl]-2-methyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

isopropylidene-[G-2]-benzyl ester (205878-77-9) → isopropylidene-[G-2]-benzyl ester (199457-34-6)

Guidance literature:

With sulfuric acid; In methanol;

DOI:10.1021/ja2070736

Reference yield:

2,2,5-trimethyl-1,3-dioxane-5-carboxylic anhydride (408322-03-2) → isopropylidene-[G-2]-benzyl ester (199457-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: DMAP / CH₂Cl₂

2: 0.3 M H₂SO₄ / methanol; H₂O

With dmap; sulfuric acid; In methanol; dichloromethane; water;

DOI:10.1021/jo011005x

Reference yield:

2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid (16837-14-2) → isopropylidene-[G-2]-benzyl ester (199457-34-6)

Guidance literature:

Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide / dichloromethane

2: dmap / dichloromethane

3: sulfuric acid / methanol

With dmap; sulfuric acid; dicyclohexyl-carbodiimide; In methanol; dichloromethane;

DOI:10.1021/ja2070736

upstream raw materials:

isopropylidene-[G-2]-benzyl ester

2,2,5-trimethyl-1,3-dioxane-5-carboxylic anhydride

2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid

benzyl 2,2-bis(hydroxylmethyl)propionate

Downstream raw materials:

C₅₀H₄₄N₄O₂₆

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