3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one

Base Information

Chemical Name:3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one
CAS No.:108361-85-9
Molecular Formula:C16H14 N2 O4 S
Molecular Weight:330.35836
Hs Code.:
Mol file:108361-85-9.mol

$3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one$

Synonyms:3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one

Suppliers and Price of 3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one

Chemical Property:

Vapor Pressure:2.46E-13mmHg at 25°C
Boiling Point:577.5°Cat760mmHg
Flash Point:303.1°C
PSA：92.79000
Density:1.403g/cm³
LogP:2.74450

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one

There total 1 articles about 3,5-dimethyl-9,9-dioxo-8-phenacyl-9$l^{6}-thia-2,8-diazabicyclo[4.3.0] nona-2,4,10-trien-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: C₈H₇N₂O₃S^(1-)*Na⁽¹⁺⁾

: 108361-85-9
2H-2-phenacyl-4,6-dimethylpyrido<3,2-d>isothiazoline-3-one-1,1-dioxide

Guidance literature:: In N,N-dimethyl-formamide; at 70 - 80 ℃; for 7h;

Reference yield: 85.0%

: 108361-85-9
2H-2-phenacyl-4,6-dimethylpyrido<3,2-d>isothiazoline-3-one-1,1-dioxide

: 108586-75-0
2H-3-benzoyl-4-hydroxy-5,7-dimethylpyrido<3,2-e>-1,2-thiazine-1,1-dioxide

Guidance literature:: With sodium; In ethanol; at 55 - 60 ℃; for 0.333333h;

Reference yield:

: 108361-85-9
2H-2-phenacyl-4,6-dimethylpyrido<3,2-d>isothiazoline-3-one-1,1-dioxide

: 108586-76-1
2H-3-benzoyl-4-hydroxy-2,5,7-trimethylpyrido<3,2-e>-1,2-thiazine-1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium / ethanol / 0.33 h / 55 - 60 °C

2: 1.2 g / 1 N KOH / H₂O / 1.) 3 h; 2.) 2 h, r.t.

With potassium hydroxide; sodium; In ethanol; water;