Carbamic acid, [(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester

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Chemical Name:Carbamic acid, [(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester
CAS No.:201006-62-4
Molecular Formula:C28H37N5O6S2
Molecular Weight:603.764
Hs Code.:

Carbamic acid,
[(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl
phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester

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Chemical Property of Carbamic acid, [(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester

There total 8 articles about Carbamic acid, [(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethyl phenyl)sulfonyl]amino]methyl]amino]butyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 95-16-9
1,3-Benzothiazole

: {(3S)-1-[imino-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-2-oxo-piperidin-3-yl}-carbamic acid tert-butyl ester

: 2386-64-3
ethylmagnesium chloride

: C₂₃H₃₈N₄SO₆

: 201006-62-4
[(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]carbamic acid 1,1-dimethylethyl ester

Guidance literature:: 1,3-Benzothiazole; With ethylmagnesium chloride; In tetrahydrofuran; at 10 ℃;

{(3S)-1-[imino-(4-methoxy-2,3,6-trimethyl-benzenesulfonylamino)-methyl]-2-oxo-piperidin-3-yl}-carbamic acid tert-butyl ester; ethylmagnesium chloride; In tetrahydrofuran; Further stages.;
DOI:10.1021/jo7019543

Reference yield: 94.0%

: 95-16-9
1,3-Benzothiazole

: 142801-55-6
N-α-(t-butyloxycarbonyl)-N'-ω'-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-L-arginine-N,O-dimethylhydroxyamide

: 201006-62-4
[(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]carbamic acid 1,1-dimethylethyl ester

Guidance literature:: 1,3-Benzothiazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

N-α-(t-butyloxycarbonyl)-N'-ω'-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-L-arginine-N,O-dimethylhydroxyamide; In tetrahydrofuran; hexane; at -78 ℃; for 2.83333h;

Reference yield: 90.0%

: 95-16-9
1,3-Benzothiazole

: 1001068-45-6
C₂₄H₃₆N₆SO₆

: 201006-62-4
[(1S)-1-(2-benzothiazolylcarbonyl)-4-[[imino[[(4-methoxy-2,3,6-trimethylphenyl)sulfonyl]amino]methyl]amino]butyl]carbamic acid 1,1-dimethylethyl ester

Guidance literature:: 1,3-Benzothiazole; With tert-butylmagnesium chloride; In tetrahydrofuran; at 6 - 8 ℃; for 0.166667h;

C₂₄H₃₆N₆SO₆; In tetrahydrofuran; at 10 ℃; for 0.25h; Further stages.;
DOI:10.1021/jo7019543