2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

Base Information

Chemical Name:2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one
CAS No.:201024-63-7
Molecular Formula:C8H9NO2
Molecular Weight:151.165
Hs Code.:
DSSTox Substance ID:DTXSID50571896
Nikkaji Number:J948.561I
Wikidata:Q82460084

Synonyms:201024-63-7;2-methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one;2-Methyl-6,7-dihydrobenzo[d]oxazol-4(5H)-one;4(5H)-Benzoxazolone, 6,7-dihydro-2-methyl-;2-METHYL-6,7-DIHYDRO-5H-1,3-BENZOXAZOL-4-ONE;SCHEMBL5367580;DTXSID50571896;BIA02463;EN300-258700;2-methyl-6,7-dihydro-1,3-benzoxazol-4(5h)-one

Suppliers and Price of 2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:151.063328530
Heavy Atom Count:11
Complexity:181

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=NC2=C(O1)CCCC2=O

Technology Process of 2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

There total 1 articles about 2-Methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 86396-02-3
2-(phenyl-λ³-iodaneylidene)cyclohexane-1,3-dione

: 75-05-8,26809-02-9
acetonitrile

: 201024-63-7
2-methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

: 2-iodo-3-phenoxycyclohex-2-enone

Guidance literature:: With copper acetylacetonate; Heating;
DOI:10.1016/S0040-4039(98)01997-2

Reference yield: 71.0%

: 1402838-08-7
2-[1-(triphenylmethyl)-1H-imidazol-4-yl]benzaldehyde

: 201024-63-7
2-methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

: (E)-2-methyl-5-(2-(1-trityl-1H-imidazol-4-yl)styryl)-6,7-dihydrobenzo[d]oxazol-4(5H)-one

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃;

Reference yield:

: 201024-63-7
2-methyl-4,5,6,7-tetrahydro-1,3-benzoxazol-4-one

: 5-(5H-imidazo[5,1-a]isoindol-5-yl)-2-methyl-4,5,6,7-tetrahydrobenzo[d]oxazol-4-yl 4-nitrobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / -78 - 20 °C

2: acetic acid / methanol / 2 h / 80 °C

3: L-Selectride / tetrahydrofuran / 0.5 h / -78 °C

4: tributylphosphine; di-tert-butyl-diazodicarboxylate / tetrahydrofuran / 20 °C

With n-butyllithium; tributylphosphine; di-tert-butyl-diazodicarboxylate; L-Selectride; acetic acid; diisopropylamine; In tetrahydrofuran; methanol; hexane;