Di(pentafluorophenyl)dichlorosilane

Base Information

• Chemical Name: Di(pentafluorophenyl)dichlorosilane
• CAS No.: 20160-45-6
• Molecular Formula: C12Cl2F10Si
• Molecular Weight: 433.108
• DSSTox Substance ID: DTXSID30455620
• Wikidata: Q82277710
• Mol file: 20160-45-6.mol

Synonyms:di(pentafluorophenyl)dichlorosilane;20160-45-6;SCHEMBL3141756;DTXSID30455620;FKCZWZMIVZFKBK-UHFFFAOYSA-N;dichlorobis(pentafluorophenyl)silane

Chemical Property of Di(pentafluorophenyl)dichlorosilane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 10
• Rotatable Bond Count: 2
• Exact Mass: 431.8986635
• Heavy Atom Count: 25
• Complexity: 415

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1(=C(C(=C(C(=C1F)F)[Si](C2=C(C(=C(C(=C2F)F)F)F)F)(Cl)Cl)F)F)F

Technology Process of Di(pentafluorophenyl)dichlorosilane

There total 7 articles about Di(pentafluorophenyl)dichlorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

di-(pentafluoro phenyl) diphenyl silane (17067-70-8) → bis-(pentafluoro phenyl) dichloro silane (20160-45-6)

Guidance literature:

With aluminium trichloride; In chloroform; for 0.25h; Ambient temperature;

DOI:10.1016/S0022-328X(98)00720-7

Reference yield: 64.0%

bis-(pentafluoro phenyl) diethoxy silane (13888-69-2) → bis-(pentafluoro phenyl) dichloro silane (20160-45-6)

Guidance literature:

With thionyl chloride; pyridine hydrochloride; for 24h; Heating;

DOI:10.1016/0022-328X(95)05676-G

Reference yield:

bromopentafluorobenzene (344-04-7) → bis-(pentafluoro phenyl) dichloro silane (20160-45-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) ether, hexane, -78 deg C, 1 h, 2.) ether, hexane, -78 deg C, then room t.

2: 100 percent / AlCl₃ / CHCl₃ / 0.25 h / Ambient temperature

With n-butyllithium; aluminium trichloride; In chloroform;

DOI:10.1016/S0022-328X(98)00720-7

upstream raw materials:

bis-(pentafluoro phenyl) diethoxy silane

di-(pentafluoro phenyl) diphenyl silane

bromopentafluorobenzene

acetyl chloride

Downstream raw materials:

bis-(pentafluoro phenyl) diethoxy silane