3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride

Base Information

Chemical Name:3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride
CAS No.:60450-40-0
Molecular Formula:C14H13ClO
Molecular Weight:232.71
Hs Code.:2916399090
European Community (EC) Number:262-237-8
DSSTox Substance ID:DTXSID50975855
Nikkaji Number:J268.197H
Mol file:60450-40-0.mol

Synonyms:60450-40-0;3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride;EINECS 262-237-8;3,3-dimethylspiro[cyclopropane-1,1'-[1H]indene]-2-carbonyl chloride;3,3-dimethylspiro[cyclopropane-1,1'-indene]-2-carbonyl chloride;SCHEMBL11158330;DTXSID50975855;3,3-dimethyl-spiro(cyclopropane-1,1'-indene)-2-carboxylic acid chloride;3,3-dimethylspiro-(cyclopropane-1,1'-indene)-2-carboxylic acid chloride;3,3-Dimethylspiro[cyclopropane-1,1'-[1H]indene]-2-carboxylic acid chloride;3,3-dimethylspiro[cyclopropane-1,1'-indene]-2-carboxylic acid chloride

Suppliers and Price of 3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride

Chemical Property:

Boiling Point:323.7oC at 760 mmHg
Flash Point:190oC
PSA：17.07000
Density:1.24g/cm3
LogP:3.37260
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:232.0654927
Heavy Atom Count:16
Complexity:371

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(C12C=CC3=CC=CC=C23)C(=O)Cl)C

Technology Process of 3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride

There total 3 articles about 3,3-Dimethylspiro(cyclopropane-1,1'-(1H)indene)-2-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60424-44-4
3,3-dimethylspiro(cyclopropane-1,1'-[1H]indene)-2-carboxylic acid

: 60450-40-0
3,3-dimethyl-spiro(cyclopropane-1,1'-indene)-2-carboxylic acid chloride

Guidance literature:: With thionyl chloride; In benzene; 1.) 25 deg C, 12 h, 2.) reflux, 20 min;

Reference yield:

: 65540-54-7
ethyl 3,3-dimethylspiro-2-carboxylate

: 60450-40-0
3,3-dimethyl-spiro(cyclopropane-1,1'-indene)-2-carboxylic acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: aq. potassium hydroxide / ethanol / 2 h / 60 °C

2: thionyl chloride / benzene / 1.) 25 deg C, 12 h, 2.) reflux, 20 min

With potassium hydroxide; thionyl chloride; In ethanol; benzene;