2-octylpropane-1,3-diol

Base Information

• Chemical Name: 2-octylpropane-1,3-diol
• CAS No.: 74971-70-3
• Molecular Formula: C11H24 O2
• Molecular Weight: 188.31
• Mol file: 74971-70-3.mol

Synonyms:2-(n-Octyl)-1,3-propanediol;2-Octyl-1,3-propanediol; NSC 243513

Chemical Property of 2-octylpropane-1,3-diol

Chemical Property:

• Vapor Pressure: 0.000135mmHg at 25°C
• Boiling Point: 297.7°Cat760mmHg
• Flash Point: 133.6°C
• Density: 0.916g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-octylpropane-1,3-diol

There total 6 articles about 2-octylpropane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

diethyl octylmalonate (1472-85-1) → 2-n-octylpropane-1,3-diol (74971-70-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/jo001620l

Reference yield: 65.0%

→ 2-n-octylpropane-1,3-diol (74971-70-3)

Guidance literature:

Reference yield:

1-bromo-octane (111-83-1) → 2-n-octylpropane-1,3-diol (74971-70-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / NaOEt / ethanol

2: 75 percent / LiAlH₄ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; sodium ethanolate; In tetrahydrofuran; ethanol;

DOI:10.1021/jo001620l

upstream raw materials:

diethyl octylmalonate

1-bromo-octane

diethyl malonate

Downstream raw materials:

diethyl N-benzyl-3,4-(2-octyl-1,3-propylenedioxy)pyrrole-2,5-dicarboxylate

trans 2-(p-cyanophenyl)-5-(n-octyl)-1,3-oxathiane

cis 2-(p-cyanophenyl)-5-(n-octyl)-1,3-oxathiane

2,14-di-(n-octyl)-4,8,12-trioxapentadecane-1,15-ditosylate

Refernces

• 1、 Zong,Reynolds. "3,4-Alkylenedioxypyrroles: Functionalized derivatives as monomers for new electron-rich conducting and electroactive polymers". . p. 6873 - 6882. Retrieved 2007/10/03.
• 2、 -. "Dioxane derivatives". . . Retrieved 2008/06/13.