Technology Process of Acetamide, 2-chloro-N-[3-(4-chlorobenzoyl)-4,5-dimethyl-2-thienyl]-
There total 1 articles about Acetamide, 2-chloro-N-[3-(4-chlorobenzoyl)-4,5-dimethyl-2-thienyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: morpholine; sulfur / ethanol / 12 h / 70 °C / Inert atmosphere
2: chloroform / 1 h / 70 °C
With
morpholine; sulfur;
In
ethanol; chloroform;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium iodide / tetrahydrofuran / 2 h / 60 °C
2.1: ammonia / tetrahydrofuran / 3.5 h / -60 - 20 °C
3.1: acetic acid / isopropyl alcohol / 3 h / 90 °C
4.1: tetraphosphorus decasulfide; sodium carbonate / 1,2-dichloro-ethane / 5 h / 65 °C
5.1: hydrazine hydrate / methanol / 1 h / 0 °C
6.1: toluene / 1 h / 80 °C
7.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -70 °C
7.2: 5 h / -70 - 20 °C
With
tetraphosphorus decasulfide; hydrazine hydrate; ammonia; sodium carbonate; acetic acid; sodium iodide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; 1,2-dichloro-ethane; isopropyl alcohol; toluene;
- Guidance literature:
-
With
sodium iodide;
In
tetrahydrofuran;
at 60 ℃;
for 2h;
