Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-

Base Information

Chemical Name:Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-
CAS No.:204907-49-3
Molecular Formula:C17H11NO5
Molecular Weight:309.278
Hs Code.:
DSSTox Substance ID:DTXSID50439043
Wikidata:Q82254919

Synonyms:204907-49-3;Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-;SCHEMBL13380162;DTXSID50439043;2-(9,10-Dioxo-9,10-dihydroanthracene-2-carboxamido)aceticacid;2-(9,10-Dioxo-9,10-dihydroanthracene-2-carboxamido)acetic acid

Suppliers and Price of Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:309.06372245
Heavy Atom Count:23
Complexity:543

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C=C(C=C3)C(=O)NCC(=O)O

Technology Process of Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]-

There total 1 articles about Glycine, N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84-54-8
2-methylanthracene-9,10-dione

: 204907-49-3
N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine

Guidance literature:: Multi-step reaction with 4 steps

1: chromium(VI) oxide; acetic acid / 1 h / Reflux

2: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 40 °C

3: triethylamine / dichloromethane / 0 - 20 °C

4: sodium hydroxide; water / tetrahydrofuran; methanol / 4 h / 50 °C

With chromium(VI) oxide; thionyl chloride; water; acetic acid; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1111/cbdd.13156

Reference yield: 99.0%

: 956092-70-9
(2S,3S)-3-amino-4-{4,4’-dimethoxytrityloxy}butan-2-ol

: 204907-49-3
N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine

: C₄₂H₃₈N₂O₈

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1039/d0cc01865a

Reference yield: 27.0%

: 204907-49-3
N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine

: 30418-59-8,280563-63-5
3-Aminophenylboronic acid

: 1385833-45-3
C₂₃H₁₇BN₂O₆

Guidance literature:: 3-Aminophenylboronic acid; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

N-[(9,10-dihydro-9,10-dioxo-2-anthracenyl)carbonyl]glycine; With N-ethylmorpholine;; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 20h; Inert atmosphere;

With trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; for 0.0166667h; Inert atmosphere;
DOI:10.1039/c2cc33559j