3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide

Base Information

• Chemical Name: 3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide
• CAS No.: 20600-84-4
• Molecular Formula: C15H21NO
• Molecular Weight: 231.33300
• Hs Code.: 2926909090
• Mol file: 20600-84-4.mol

Synonyms:3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide;

Chemical Property of 3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide

Chemical Property:

• PSA: 20.23000
• LogP: 3.76870

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide

There total 2 articles about 3,5-Di-tert-butyl-4-hydroxyphenyl isocyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3,5-di-tert-butyl-4-hydroxybenzaldehyde oxime (787-13-3) → 3,5-di-tert-butyl-4-hydroxyphenyl isocyanide (20600-84-4)

Guidance literature:

With triethylamine; p-toluenesulfonyl chloride; In dichloromethane; at 5 - 20 ℃; for 1.5h;

DOI:10.1007/BF01457806

Reference yield:

→ 3,5-di-tert-butyl-4-hydroxyphenyl isocyanide (20600-84-4)

Guidance literature:

3.5-Di-tert.-butyl-4-hydroxy-benzaldoxim, Tosylchlorid;

Reference yield: 96.0%

3,5-di-tert-butyl-4-hydroxyphenyl isocyanide (20600-84-4) → 2,6-di-tert-butyl-4-cyanophenol (1988-88-1)

Guidance literature:

In toluene; for 1h; Heating;

DOI:10.1007/BF01457806

upstream raw materials:

3,5-di-tert-butyl-4-hydroxybenzaldehyde oxime

Downstream raw materials:

C₅₁H₇₈NO₃

2,6-di-tert-butyl-4-cyanophenol

3,5-di-tert-butyl-4-hydroxyformanilide