1,3-Benzenedicarbonitrile, 4-(phenylmethoxy)-

Base Information

Chemical Name:1,3-Benzenedicarbonitrile, 4-(phenylmethoxy)-
CAS No.:206533-18-8
Molecular Formula:C15H10N2O
Molecular Weight:234.257
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Benzenedicarbonitrile, 4-(phenylmethoxy)-

Chemical Property:

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Technology Process of 1,3-Benzenedicarbonitrile, 4-(phenylmethoxy)-

There total 7 articles about 1,3-Benzenedicarbonitrile, 4-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.1%

: 34133-58-9
4-hydroxy-isophthalonitrile

: 206533-18-8
4-benzyloxyisophthalonitrile

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; for 6h; Inert atmosphere;
DOI:10.1016/j.ejmech.2019.07.061

Reference yield: 80.1%

: 206533-18-8
4-benzyloxyisophthalonitrile

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 90-02-8
salicylaldehyde

: 206533-18-8
4-benzyloxyisophthalonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride / water / 1 h / 20 °C

1.2: 8 h

2.1: acetic acid; hexamethylenetetramine / water / 1 h / Reflux

3.1: hydroxylamine hydrochloride; sodium formate; formic acid / 1-methyl-pyrrolidin-2-one / 6 h / Reflux

4.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 6 h / Inert atmosphere

With hydrogenchloride; formic acid; hexamethylenetetramine; hydroxylamine hydrochloride; sodium formate; potassium carbonate; acetic acid; potassium iodide; In 1-methyl-pyrrolidin-2-one; water; N,N-dimethyl-formamide; 2.1: |Sommelet Aldehyde Synthesis;
DOI:10.1016/j.ejmech.2019.07.061