1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine

Base Information

Chemical Name:1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine
CAS No.:91417-79-7
Molecular Formula:C₁₁H₁₇N₃O₂
Molecular Weight:223.275
Hs Code.:

Synonyms:BRN 5537101;N-(1-(Cyanomethyl)-2-pyrrolidinylidene)-L-valine;L-Valine, N-(1-(cyanomethyl)-2-pyrrolidinylidene)-;1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine;91417-79-7;LS-161306

Suppliers and Price of 1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine

Chemical Property:

Vapor Pressure:3.21E-08mmHg at 25°C
Boiling Point:419.7°Cat760mmHg
Flash Point:207.6°C
Density:1.19g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:223.132076794
Heavy Atom Count:16
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C(=O)O)N=C1CCCN1CC#N

Technology Process of 1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine

There total 4 articles about 1-Cyanomethyl-2-(N-(1-carboxy-2,2-dimethylethyl))iminopyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 91417-88-8
diethylacetal of N-cyanomethyl-2-pyrrolidone

: 516-06-3,25609-85-2,7004-03-7,921-10-8
D,L-valine

: 91417-79-7
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: In ethanol; Ambient temperature;
DOI:10.1007/BF00758995

Reference yield:

: 57275-83-9
nitrile of 2-oxopyrrolidine-1-acetic acid

: 91417-79-7
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) POCl₃ / 1.) benzene, room temp., 4.5 h, 2.) EtOH, 0.5 h

2: 72 percent / ethanol / Ambient temperature

With trichlorophosphate; In ethanol;
DOI:10.1007/BF00758995

Reference yield:

: 7491-74-9
2-oxo-1-pyrrolidine acetamide

: 91417-79-7
1-Cyanomethyl-2-iminopyrrolidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) POCl₃, DMF, 2.) pyridine / 1.) acetonitrile, 50 deg C, 2.5 h, 2.) 0 deg C, 20 min

2: 1.) POCl₃ / 1.) benzene, room temp., 4.5 h, 2.) EtOH, 0.5 h

3: 72 percent / ethanol / Ambient temperature

With pyridine; N,N-dimethyl-formamide; trichlorophosphate; In ethanol;
DOI:10.1007/BF00758995