1H-Indene-1,3(2H)-dione, dihydrazone

Base Information

• Chemical Name: 1H-Indene-1,3(2H)-dione, dihydrazone
• CAS No.: 21040-05-1
• Molecular Formula: C9H10N4
• Molecular Weight: 174.205
• DSSTox Substance ID: DTXSID10408472

Synonyms:1,3-indanedione dihydrazone;1H-Indene-1,3(2H)-dione, dihydrazone;21040-05-1;DTXSID10408472

Chemical Property of 1H-Indene-1,3(2H)-dione, dihydrazone

Chemical Property:

• XLogP3: 1.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 174.090546336
• Heavy Atom Count: 13
• Complexity: 230

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(=NN)C2=CC=CC=C2C1=NN

Technology Process of 1H-Indene-1,3(2H)-dione, dihydrazone

There total 1 articles about 1H-Indene-1,3(2H)-dione, dihydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Acetyl-2-methyl-4-phenyl-5-oxo-4,5-dihydro-1H-indeno<1,2-b>pyridine (26576-80-7) → 3,5-dimethyl-4-[α-(1,3-dihydrazono-2-indanyl)benzyl]pyrazole + 1,3-dihydrazono-2,3-dihydro-1H-indene (21040-05-1)

Guidance literature:

With hydrazine hydrate; In ethanol; at 140 ℃; for 6h;

DOI:10.1023/B:COHC.0000044569.14048.79

Reference yield: 95.0%

1,3-dihydrazono-2,3-dihydro-1H-indene (21040-05-1) + 1-(N-phenylhydrazono)-1-chloropropanone (18440-58-9,1017827-91-6) → 1,1'((indene-1,3(2H)-dihylidene))bis(3-acetyl-5-phenyl-1,2-dihydroformazan)

Guidance literature:

With triethylamine; In 1,4-dioxane; Reflux;

DOI:10.2174/1573406412666160920091146

Reference yield: 95.0%

1,3-dihydrazono-2,3-dihydro-1H-indene (21040-05-1) + 1-chloro-1-(p-tolylhydrazone)propanone (132815-80-6,18440-55-6) → 1,1'((indene-1,3(2H)-dihylidene))bis(3-acetyl-5-(4-methylphenyl)-1,2-dihydroformazan)

Guidance literature:

With triethylamine; In 1,4-dioxane; Reflux;

DOI:10.2174/1573406412666160920091146

upstream raw materials:

3-Acetyl-2-methyl-4-phenyl-5-oxo-4,5-dihydro-1H-indeno<1,2-b>pyridine

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