Benzaldehyde, 3-acetyl-2,4-dihydroxy-

Base Information

Chemical Name:Benzaldehyde, 3-acetyl-2,4-dihydroxy-
CAS No.:213916-38-2
Molecular Formula:C9H8O4
Molecular Weight:180.15700
Hs Code.:
Mol file:213916-38-2.mol

Synonyms:3-acetyl-2,4-dihydroxy-benzaldehyde;Benzaldehyde,3-acetyl-2,4-dihydroxy;3-acetyl-2,4-dihydroxybenzalodehyde;3-Acetyl-2,4-dihydroxy-benzaldehyd;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 3-acetyl-2,4-dihydroxy-

Chemical Property:

Melting Point:105-106 °C
Boiling Point:289.9±40.0 °C(Predicted)
PSA：74.60000
Density:1.391±0.06 g/cm3(Predicted)
LogP:1.11290

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Benzaldehyde, 3-acetyl-2,4-dihydroxy-

There total 3 articles about Benzaldehyde, 3-acetyl-2,4-dihydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 287942-42-1
1-(2’,6’-dihydroxy-3’-(3’’-methyl-2’’-buten-1’’-yl)phenyl)ethanone

: 213916-38-2
3-acetyl-2,4-dihydroxybenzalodehyde

: 1-[2,6-dihydroxy-3-(2-hydroxy-3-methylbut-3-enyl)phenyl]ethanone

Guidance literature:: 1-(2’,6’-dihydroxy-3’-(3’’-methyl-2’’-buten-1’’-yl)phenyl)ethanone; With air; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at 15 ℃; for 1.5h; Irradiation;

With triphenylphosphine; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1016/S0040-4020(03)00733-6

Reference yield:

: 699-83-2
2,6-dihydroxylacetophenone

: 213916-38-2
3-acetyl-2,4-dihydroxybenzalodehyde

Guidance literature:: With hydrogenchloride; diethyl ether; Erwaermen des Reaktionsprodukts mit Wasser;
DOI:10.1039/jr9390000949

Reference yield:

: 699-83-2
2,6-dihydroxylacetophenone

: 213916-38-2
3-acetyl-2,4-dihydroxybenzalodehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: 42 percent / BF₃*Et₂O / dioxane / 48 h / 20 °C

2.1: air; tetraphenylporphine / CH₂Cl₂ / 1.5 h / 15 °C / Irradiation

2.2: 16 percent / triphenylphosphine / CH₂Cl₂ / 15 h / 20 °C

With air; boron trifluoride diethyl etherate; 5,15,10,20-tetraphenylporphyrin; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0040-4020(03)00733-6