1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride

Base Information

Chemical Name:1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride
CAS No.:134285-32-8
Molecular Formula:C₂₀H₁₆N₂*ClH
Molecular Weight:320.821
Hs Code.:
DSSTox Substance ID:DTXSID10158627

Synonyms:8-Phenyl-2,3-dihydro-1H-pyrazino(3,2,l-jk)carbazole hydrochloride;1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride;134285-32-8;DTXSID10158627;LS-127660

Suppliers and Price of 1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of 1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride

Chemical Property:

Vapor Pressure:2.62E-12mmHg at 25°C
Boiling Point:553.8°C at 760 mmHg
Flash Point:288.8°C
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:320.1080262
Heavy Atom Count:23
Complexity:403

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CN2C3=C(C=C(C=C3)C4=CC=CC=C4)C5=C2C(=CC=C5)N1.Cl

Technology Process of 1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride

There total 4 articles about 1H-Pyrazino(3,2,1-jk)carbazole, 2,3-dihydro-8-phenyl-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134285-24-8
6-phenyl-1-keto-1,2,3,4-tetrahydrocarbazole

: 134285-32-8
8-phenyl-2,3-dihydro-1H-pyrazino<3,2,1-jk>carbazole hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / xylene / 4 h / Heating

2: 67 percent / thionyl chloride / benzene; dimethylformamide / 1 h / 70 - 76 °C

3: 1.) NaBH₄, 2.) tetrabutylammonium bromide, NaOH / 1.) ethanol, 0 deg C, 1 h, 2.) benzene, water, RT, 5 h

4: 2.) HCl / 1.) Pd/C / 1.) xylene, RT, 2.) ethanol

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; tetrabutylammomium bromide; palladium on activated charcoal; In N,N-dimethyl-formamide; xylene; benzene;
DOI:10.1007/BF00766565

Reference yield:

: 1-(2-hydroxyethylimino)-6-phenyl-1,2,3,4-tetrahydrocarbazole

: 134285-32-8
8-phenyl-2,3-dihydro-1H-pyrazino<3,2,1-jk>carbazole hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / thionyl chloride / benzene; dimethylformamide / 1 h / 70 - 76 °C

2: 1.) NaBH₄, 2.) tetrabutylammonium bromide, NaOH / 1.) ethanol, 0 deg C, 1 h, 2.) benzene, water, RT, 5 h

3: 2.) HCl / 1.) Pd/C / 1.) xylene, RT, 2.) ethanol

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; tetrabutylammomium bromide; palladium on activated charcoal; In N,N-dimethyl-formamide; benzene;
DOI:10.1007/BF00766565

Reference yield:

: 134285-27-1
8-phenyl-2,3,3a,4,5,6-hexahydro-1H-pyrazino<3,2,1-jk>carbazole

: 134285-32-8
8-phenyl-2,3-dihydro-1H-pyrazino<3,2,1-jk>carbazole hydrochloride

Guidance literature:: With hydrogenchloride; palladium on activated charcoal; Yield given. Multistep reaction; 1.) xylene, RT, 2.) ethanol;
DOI:10.1007/BF00766565