Cyclohexene, 6,6-difluoro-1-iodo-

Base Information

Chemical Name:Cyclohexene, 6,6-difluoro-1-iodo-
CAS No.:218629-47-1
Molecular Formula:C6H7F2I
Molecular Weight:244.023
Hs Code.:
DSSTox Substance ID:DTXSID80448901
Nikkaji Number:J874.727J
Wikidata:Q82268099
Mol file:218629-47-1.mol

Synonyms:Cyclohexene, 6,6-difluoro-1-iodo-;218629-47-1;SCHEMBL5475189;1-Iodo-6,6-difluorocyclohexene;DTXSID80448901;VHOJXLXCUXNEDO-UHFFFAOYSA-N

Suppliers and Price of Cyclohexene, 6,6-difluoro-1-iodo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclohexene, 6,6-difluoro-1-iodo-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:243.95605
Heavy Atom Count:9
Complexity:140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=C(C(C1)(F)F)I

Technology Process of Cyclohexene, 6,6-difluoro-1-iodo-

There total 2 articles about Cyclohexene, 6,6-difluoro-1-iodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33948-36-6
2-iodocyclohex-2-en-1-one

: 2,6-difluoro-1-iodocyclohexene

: 218629-47-1
6,6-difluoro-1-iodocyclohex-1-ene

Guidance literature:: With morpholinosulfur trifluoride; In dichloromethane; at 40 ℃; for 72h; under 14251100 Torr; Yield given. Yields of byproduct given;
DOI:10.1055/s-1997-3224

Reference yield:

: 33948-36-6
2-iodocyclohex-2-en-1-one

: 218629-47-1
6,6-difluoro-1-iodocyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: morpholino-SF₃ / CH₂Cl₂ / 72 h / 40 °C / 7500600 Torr

2: molecular sieves 4 Angstroem / CH₂Cl₂ / 8 h

With 4 A molecular sieve; morpholinosulfur trifluoride; In dichloromethane;
DOI:10.1055/s-1997-3224

Reference yield: 96.0%

: 218629-47-1
6,6-difluoro-1-iodocyclohex-1-ene

: 98-80-6
phenylboronic acid

: 6,6-difluoro-1-phenylcyclohex-1-ene

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; lithium chloride; In 1,2-dimethoxyethane; water; for 15h; Heating;
DOI:10.1016/S0040-4020(03)00697-5