9,10-Didehydro-6-methylergolin-8alpha-amine

Base Information

Chemical Name:9,10-Didehydro-6-methylergolin-8alpha-amine
CAS No.:58084-48-3
Molecular Formula:C15H17 N3
Molecular Weight:239.32
Hs Code.:
European Community (EC) Number:261-104-1
DSSTox Substance ID:DTXSID80206806
Nikkaji Number:J296.865G
Wikidata:Q83080658

Synonyms:9,10-Didehydro-6-methylergolin-8alpha-amine;58084-48-3;EINECS 261-104-1;(6aR,9S)-7-Methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-amine;SCHEMBL7265357;DTXSID80206806;YFPQZLKFHUVMEA-IINYFYTJSA-N;8alpha-amino-6-methyl-9,10-didehydro-ergoline

Suppliers and Price of 9,10-Didehydro-6-methylergolin-8alpha-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 12 raw suppliers

Chemical Property of 9,10-Didehydro-6-methylergolin-8alpha-amine

Chemical Property:

Boiling Point:454.9°Cat760mmHg
Flash Point:228.9°C
Density:1.29g/cm³
XLogP3:1.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:239.142247555
Heavy Atom Count:18
Complexity:378

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CC(C=C2C1CC3=CNC4=CC=CC2=C34)N
Isomeric SMILES:CN1C[C@H](C=C2[C@H]1CC3=CNC4=CC=CC2=C34)N

Technology Process of 9,10-Didehydro-6-methylergolin-8alpha-amine

There total 5 articles about 9,10-Didehydro-6-methylergolin-8alpha-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 55584-33-3
N-(6-methyl-9,10-didehydro-ergolin-8α-yl)-acetamide

: 58084-48-3
(5R,8S)-8-Amino-6-methyl-9,10-didehydro-ergolin

Guidance literature:: With hydrogenchloride; In water; for 11h; Inert atmosphere; Reflux;

Reference yield:

: 18016-80-3,36307-98-9,107492-84-2,107596-79-2,140387-89-9
lisuride

: 58084-48-3
(5R,8S)-8-Amino-6-methyl-9,10-didehydro-ergolin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.83 h / 133 °C / Inert atmosphere

2: hydrogenchloride / water / 11 h / Inert atmosphere; Reflux

With hydrogenchloride; In water;

Reference yield:

: 5256-60-0
6-methyl-9,10-didehydro-ergoline-8-carboxylic acid hydrazide

: 58084-48-3
(5R,8S)-8-Amino-6-methyl-9,10-didehydro-ergolin

Guidance literature:: Multi-step reaction with 2 steps

1: water; NaNO₂; HCl

With hydrogenchloride; water; sodium nitrite;
DOI:10.1002/hlca.19470300108