5-CHLORO-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBONITRILE

Base Information

• Chemical Name: 5-CHLORO-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBONITRILE
• CAS No.: 219568-17-9
• Molecular Formula: C6H3ClF3N3
• Molecular Weight: 209.55600
• Hs Code.: 2933199090
• Mol file: 219568-17-9.mol

Synonyms:Thiocyanic acid,4-acetyl-5-(benzoylamino)-2-chlorophenyl ester;5-Chloro-4-cyanato-2-benzamidoacetophenon;5-chloro-4-cyano-1-methyl-3-trifluoromethylpyrazole;

Chemical Property of 5-CHLORO-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBONITRILE

Chemical Property:

• Melting Point: 84-86°C
• PSA: 41.61000
• LogP: 1.96398

Purity/Quality:

98%min ^*data from raw suppliers

5-Chloro-1-methyl-3-(trifluoromethyl)-1h-pyrazole-4-carbonitrile ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBONITRILE

There total 1 articles about 5-CHLORO-1-METHYL-3-(TRIFLUOROMETHYL)-1H-PYRAZOLE-4-CARBONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

5-chloro-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carbaldehyde (128455-62-9) → 5-chloro-4-cyano-1-methyl-3-trifluoromethylpyrazole (219568-17-9)

Guidance literature:

With ammonia; oxygen; In tert-Amyl alcohol; at 40 ℃; for 24h; under 750.075 Torr; Green chemistry;

DOI:10.1039/c7gc02627g

Reference yield:

5-chloro-4-cyano-1-methyl-3-trifluoromethylpyrazole (219568-17-9) → 5-chloro-4-cyanoacetyl-1-methyl-3-trifluoromethylpyrazole

Guidance literature:

With hydrogenchloride; In diethyl ether; chloroform; acetonitrile; tert-butyl alcohol;

upstream raw materials:

5-chloro-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carbaldehyde

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