Technology Process of 2,4,6,8,9,10-Hexaoxa-1,3,5,7-tetraarsatricyclo[3.3.1.13,7]decane
There total 1 articles about 2,4,6,8,9,10-Hexaoxa-1,3,5,7-tetraarsatricyclo[3.3.1.13,7]decane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
neat (no solvent);
glass pumped; purified O2 introduced; sealed; heated slowly to 650°C; homogenized at 650°C for 7 h; cooled to 400°C; transferred to another furnace (200°C) vertically; undissolved oxides condensed at cold end; detd. by absorption spectra;
DOI:10.1023/A:1012513629483
- Guidance literature:
-
In
not given;
byproducts: As, H2, H2O; refluxing for 1/2 h;;
DOI:10.1021/ja01575a023