2'-iodo-2'-deoxyadenosine

Base Information

Chemical Name:2'-iodo-2'-deoxyadenosine
CAS No.:68775-04-2
Molecular Formula:C₁₀H₁₂IN₅O₃
Molecular Weight:377.141
Hs Code.:
Mol file:68775-04-2.mol

Synonyms:2'-Ioddesoxyadenosin;2-Daio;2'-Deoxy-2'-iodoadenosine;2'-iodo-2'-deoxy-adenosine;2'-Iod-2'-deoxy-adenosin;Adenosine,2'-deoxy-2'-iodo;

Suppliers and Price of 2'-iodo-2'-deoxyadenosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2'-iodo-2'-deoxyadenosine

Chemical Property:

Boiling Point:685.4°Cat760mmHg
Flash Point:368.3°C
PSA：119.31000
Density:2.53g/cm³
LogP:0.04390

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2'-iodo-2'-deoxyadenosine

There total 6 articles about 2'-iodo-2'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 169968-53-0
2'-deoxy-2'-iodo-3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-adenosine

: 68775-04-2
2'-deoxy-2'-iodoadenosine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1080/07328319908045600

Reference yield:

: 87792-02-7
9-[3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-β-D-arabinofuranosyl]adenine

: 68775-04-2
2'-deoxy-2'-iodoadenosine

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / Et₃N, DMAP / CH₂Cl₂ / 0.83 h / Ambient temperature

2: 79 percent / LiI / hexamethylphosphoric acid triamide / 24 h / Ambient temperature

3: 83 percent / TBAF / tetrahydrofuran / 0.5 h / Ambient temperature

With dmap; tetrabutyl ammonium fluoride; triethylamine; lithium iodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1080/07328319908045600

Reference yield:

: 88121-25-9
9-[3′,5′-O-(1,1,3,3-tetraisopropyldisiloxyl)-2′-O-trifluormethylsulfonyl-β-D-arabinofuranosyl]adenine

: 68775-04-2
2'-deoxy-2'-iodoadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / LiI / hexamethylphosphoric acid triamide / 24 h / Ambient temperature

2: 83 percent / TBAF / tetrahydrofuran / 0.5 h / Ambient temperature

With tetrabutyl ammonium fluoride; lithium iodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1080/07328319908045600