Boranthrene, 1,2,3,4,6,7,8,9-octafluoro-5,10-dihydro-5,10-bis(pentafluorophenyl)-

Base Information

Chemical Name:Boranthrene, 1,2,3,4,6,7,8,9-octafluoro-5,10-dihydro-5,10-bis(pentafluorophenyl)-
CAS No.:220503-31-1
Molecular Formula:C24B2F18
Molecular Weight:651.857
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boranthrene, 1,2,3,4,6,7,8,9-octafluoro-5,10-dihydro-5,10-bis(pentafluorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Boranthrene, 1,2,3,4,6,7,8,9-octafluoro-5,10-dihydro-5,10-bis(pentafluorophenyl)-

There total 5 articles about Boranthrene, 1,2,3,4,6,7,8,9-octafluoro-5,10-dihydro-5,10-bis(pentafluorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 801-79-6
dimethylbis(pentafluorophenyl)tin

: 9,10-dichloro-1,2,3,4,5,6,7,8-octafluoro-9,10-dihydro-9,10-dibora-anthracene

: 220503-31-1
9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene

Guidance literature:: In toluene; at 140 ℃; for 72h;
DOI:10.1002/(SICI)1521-3773(20000403)39:7<1312::AID-ANIE1312>3.0.CO;2-4

Reference yield: 80.0%

: 801-79-6
dimethylbis(pentafluorophenyl)tin

: 9,10-dichloro-1,2,3,4,5,6,7,8-octafluoro-9,10-dihydro-9,10-dibora-anthracene

: 1,2-bis(dichloroboryl)tetrafluorobenzene

: 220503-31-1
9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene

Guidance literature:: In toluene; byproducts: (CH3)2SnCl2; toluene was condensed at -78°C into a tube with compounds, evacuated, the mixt. was heated to 140°C for 72 h, cooled to room temp.(N2); solbent was removed under vac., Me2SnCl2 was removed under dynamic vac. (1E-5Torr/12 h), recrystd. from toluene (slow cooling to -78°C); elem. anal.;
DOI:10.1021/om020079b

Reference yield:

: 23653-79-4
1,2-bis(trimethylstannyl)-3,4,5,6-tetrafluorobenzene

: 220503-31-1
9,10-bis(pentafluorophenyl)perfluoro-9,10-diboraanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / BCl₃ / 18 h / 180 °C

2: 80 percent / toluene / 72 h / 140 °C

With boron trichloride; In toluene; 1: Cyclization / 2: Arylation;
DOI:10.1002/(SICI)1521-3773(20000403)39:7<1312::AID-ANIE1312>3.0.CO;2-4