2-Propen-1-one, 1-(1-hydroxycyclohexyl)-

Base Information

Chemical Name:2-Propen-1-one, 1-(1-hydroxycyclohexyl)-
CAS No.:22082-46-8
Molecular Formula:C9H14O2
Molecular Weight:154.209
Hs Code.:
DSSTox Substance ID:DTXSID70393032
Nikkaji Number:J636.092K
Wikidata:Q82191633
Mol file:22082-46-8.mol

Synonyms:2-Propen-1-one, 1-(1-hydroxycyclohexyl)-;22082-46-8;SCHEMBL11025310;DTXSID70393032;1-(1-Hydroxycyclohexyl)-2-propen-1-one

Suppliers and Price of 2-Propen-1-one, 1-(1-hydroxycyclohexyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Propen-1-one, 1-(1-hydroxycyclohexyl)-

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:154.099379685
Heavy Atom Count:11
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC(=O)C1(CCCCC1)O

Technology Process of 2-Propen-1-one, 1-(1-hydroxycyclohexyl)-

There total 9 articles about 2-Propen-1-one, 1-(1-hydroxycyclohexyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 161607-26-7
2-Ethoxy-2-vinyl-1-oxaspiro<2.5>octane

: 22082-46-8
1-(1'-hydroxycyclohexyl)-2-propen-1-one

Guidance literature:: With silica gel; In diethyl ether; hexane;
DOI:10.1021/jo00128a036

Reference yield:

: 161607-25-6
1-<1-(Benzotriazol-1-yl)-1-ethoxyprop-2-enyl>cyclohexanol

: 22082-46-8
1-(1'-hydroxycyclohexyl)-2-propen-1-one

Guidance literature:: With oxalic acid; silica gel; In dichloromethane; water; for 0.0833333h; Yield given;
DOI:10.1021/jo00128a036

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 22082-46-8
1-(1'-hydroxycyclohexyl)-2-propen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 10 min, 2.) -78 deg C, 3 h; 20 deg C, 10 h

2: SiO₂, H₂C₂O₄ / CH₂Cl₂; H₂O / 0.08 h

With n-butyllithium; oxalic acid; silica gel; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo00128a036