2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-

Base Information

Chemical Name:2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-
CAS No.:223130-58-3
Molecular Formula:C19H15N3O2S2
Molecular Weight:381.479
Hs Code.:
DSSTox Substance ID:DTXSID70464236
Nikkaji Number:J1.106.926F
Wikidata:Q82289489

Synonyms:2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-;223130-58-3;DTXSID70464236

Suppliers and Price of 2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:381.06056908
Heavy Atom Count:26
Complexity:463

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)NC(=O)C2=NC(=CC=C2)C(=O)NC3=CC=CC=C3S)S

Technology Process of 2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)-

There total 5 articles about 2,6-Pyridinedicarboxamide, N,N'-bis(2-mercaptophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 341502-37-2
pyridine-2,6-dicarboxylic acid bis-[(2-tritylsulfanyl-phenyl)-amide]

: 223130-58-3
N,N'-bis(2-mercaptophenyl)pyridine-2,6-dicarboxamide

Guidance literature:: With triethylsilane; trifluoroacetic acid; In dichloromethane; for 0.25h;
DOI:10.1021/ja001253v

Reference yield: 91.0%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 137-07-5
2-amino-benzenethiol

: 223130-58-3
N,N'-bis(2-mercaptophenyl)pyridine-2,6-dicarboxamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃;
DOI:10.1081/SCC-120020209

Reference yield:

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 223130-58-3
N,N'-bis(2-mercaptophenyl)pyridine-2,6-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Et₃N / CHCl₃ / 48 h / 20 °C

2: 94 percent / Et₃SiH; TFA / CH₂Cl₂ / 0.25 h

With triethylsilane; triethylamine; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/ja001253v