2,4-Thiazolidinedione, 5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride

Base Information

Chemical Name:2,4-Thiazolidinedione, 5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride
CAS No.:223131-95-1
Molecular Formula:C29H29N3O5S.ClH
Molecular Weight:568.093
Hs Code.:

2,4-Thiazolidinedione,
5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid
azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride

Synonyms:

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Chemical Property of 2,4-Thiazolidinedione, 5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride

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Technology Process of 2,4-Thiazolidinedione, 5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride

There total 3 articles about 2,4-Thiazolidinedione, 5-[[4-[[6-[2-(1,1-dimethylethyl)-4-hydroxyphenoxy]-1-methyl-1H-benzimid azol-2-yl]methoxy]phenyl]methyl]-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: t-Butyl N-{2-[4-(2,4-dioxothiazolidin-5-ylmethyl)phenoxyacetylamino]-5-(2-t-butyl-4-hydroxyphenoxy)phenyl}-N-methylcarbamate

: 223131-95-1
5-{4-[6-(2-t-Butyl-4-hydroxyphenoxy)-1-methyl-1H-benzimidazole-2-ylmethoxy]benzyl}thiazolidine-2,4-dione hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; ethyl acetate;

Reference yield:

: 223133-57-1
t-butyl N-[5-(2-t-butyl-4-hydroxyphenoxy)-2-nitrophenyl]-N-methylcarbamate

: 223131-95-1
5-{4-[6-(2-t-Butyl-4-hydroxyphenoxy)-1-methyl-1H-benzimidazole-2-ylmethoxy]benzyl}thiazolidine-2,4-dione hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: palladium / methanol

2: triethylamine / tetrahydrofuran

3: hydrogenchloride / 1,4-dioxane; ethyl acetate

With hydrogenchloride; triethylamine; palladium; In tetrahydrofuran; 1,4-dioxane; methanol; ethyl acetate;

Reference yield:

: 223133-80-0
t-butyl N-[2-amino-5-(2-t-butyl-4-hydroxyphenoxy)phenyl]-N-methyl-carbamate

: 223131-95-1
5-{4-[6-(2-t-Butyl-4-hydroxyphenoxy)-1-methyl-1H-benzimidazole-2-ylmethoxy]benzyl}thiazolidine-2,4-dione hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran

2: hydrogenchloride / 1,4-dioxane; ethyl acetate

With hydrogenchloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethyl acetate;