1,3-Benzenedisulfonyl dichloride, 5-acetyl-

Base Information

Chemical Name:1,3-Benzenedisulfonyl dichloride, 5-acetyl-
CAS No.:225650-80-6
Molecular Formula:C8H6Cl2O5S2
Molecular Weight:317.171
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Benzenedisulfonyl dichloride, 5-acetyl-

Chemical Property:

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Technology Process of 1,3-Benzenedisulfonyl dichloride, 5-acetyl-

There total 5 articles about 1,3-Benzenedisulfonyl dichloride, 5-acetyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 335274-52-7
S-acetophenone 3,5-bis(N,N'-diethylthiocarbamate)

: 225650-80-6
3,5-bis(chlorosulfonyl)-1-acetophenone

Guidance literature:: With formic acid; water; chlorine; In dichloromethane; at 0 ℃; for 0.0333333h;
DOI:10.1021/jo001694x

Reference yield:

: 335274-53-8
3,5-bis(thiobenzyl)-1-acetophenone

: 225650-80-6
3,5-bis(chlorosulfonyl)-1-acetophenone

Guidance literature:: With formic acid; water; chlorine; In dichloromethane; at 0 ℃; for 0.0333333h;
DOI:10.1021/jo001694x

Reference yield:

: 51863-60-6
3,5-dihydroxyacetophenone

: 225650-80-6
3,5-bis(chlorosulfonyl)-1-acetophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 3 h / -5 °C

1.2: 40 percent / dimethylformamide / 2 h / 20 °C

2.1: 84 percent / 1 h / 240 °C

3.1: 77 percent / Cl₂; HCOOH; H₂O / CH₂Cl₂ / 0.03 h / 0 °C

With formic acid; water; chlorine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; 2.1: Newman-Kwart rearrangement;
DOI:10.1021/jo001694x