(2-Thiazolin-2-ylthio)acetic acid methyl ester

Base Information

• Chemical Name: (2-Thiazolin-2-ylthio)acetic acid methyl ester
• CAS No.: 22623-64-9
• Molecular Formula: C6H9NO2S2
• Molecular Weight: 191.27100
• Mol file: 22623-64-9.mol

Synonyms:(4,5-dihydro-thiazol-2-ylsulfanyl)-acetic acid methyl ester;Methyl 2-[2-thiazolin-2-ylthio]acetate;Methyl (4,5-dihydro-1,3-thiazol-2-ylsulfanyl)acetate;Acetic acid,[(4,5-dihydro-2-thiazolyl)thio]-,methyl ester;2-[(4,5-Dihydro-2-thiazolyl)thio]acetic acid methyl ester;

Chemical Property of (2-Thiazolin-2-ylthio)acetic acid methyl ester

Chemical Property:

• Boiling Point: 289℃
• Flash Point: 128℃
• PSA: 89.26000
• Density: 1.39
• LogP: 0.43100

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: thiazolidin e thione pharmaceutical intermediate

Technology Process of (2-Thiazolin-2-ylthio)acetic acid methyl ester

There total 3 articles about (2-Thiazolin-2-ylthio)acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

thallium salt of Δ2-1,3-thiazoline-2-thiol (63987-96-2) + bromoacetic acid methyl ester (96-32-2) → Δ2-Thiazolinyl-(2)-mercaptoessigsaeure-methylester (22623-64-9)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1039/P19810000914

Reference yield:

thiazolidine-2-thione (134469-06-0) + bromoacetic acid methyl ester (96-32-2) → Δ2-Thiazolinyl-(2)-mercaptoessigsaeure-methylester (22623-64-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jm00312a607

Reference yield:

→ Δ2-Thiazolinyl-(2)-mercaptoessigsaeure-methylester (22623-64-9)

Guidance literature:

Bromessigester, Mercaptothiazolin;

DOI:10.1016/S0040-4039(01)83044-6

upstream raw materials:

thiazolidine-2-thione

bromoacetic acid methyl ester

thallium salt of Δ²-1,3-thiazoline-2-thiol

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