1-(2-Bromoethoxy)dodecane

Base Information

• Chemical Name: 1-(2-Bromoethoxy)dodecane
• CAS No.: 22732-79-2
• Molecular Formula: C14H29BrO
• Molecular Weight: 293.288
• DSSTox Substance ID: DTXSID00511601
• Wikidata: Q82370475
• Mol file: 22732-79-2.mol

Synonyms:1-(2-BROMOETHOXY)DODECANE;dodecyloxyethyl bromide;22732-79-2;DTXSID00511601

Chemical Property of 1-(2-Bromoethoxy)dodecane

Chemical Property:

• XLogP3: 6.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 13
• Exact Mass: 292.14018
• Heavy Atom Count: 16
• Complexity: 117

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCOCCBr

Technology Process of 1-(2-Bromoethoxy)dodecane

There total 1 articles about 1-(2-Bromoethoxy)dodecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylene glycol mono-n-dodecyl ether (4536-30-5,9015-55-8) → 2-bromoethyl n-dodecyl ether (22732-79-2) + 1-dodecylbromide (143-15-7)

Guidance literature:

With pyridine; phosphorus tribromide; at -10 - 25 ℃; for 2h;

DOI:10.1007/s11172-014-0761-x

Reference yield:

2-bromoethyl n-dodecyl ether (22732-79-2) + 3-benzyloxypropan-1,2-diol (13071-59-5,17325-85-8,56552-80-8,4799-67-1) → 17-Benzyloxymethyl-13,16,19,22-tetraoxatetratriacontan (87117-78-0)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1) 30 min, r. t., THF, 2) 6 h, reflux, THF;

upstream raw materials:

ethylene glycol mono-n-dodecyl ether

Downstream raw materials:

17-Benzyloxymethyl-13,16,19,22-tetraoxatetratriacontan