1,5,9-Triphenyl-1,5,9-triphosphacyclododecane

Base Information

Chemical Name:1,5,9-Triphenyl-1,5,9-triphosphacyclododecane
CAS No.:227605-73-4
Molecular Formula:C₂₇H₃₃P₃
Molecular Weight:450.48
Hs Code.:
DSSTox Substance ID:DTXSID30436515
Nikkaji Number:J1.091.782D
Mol file:227605-73-4.mol

Synonyms:1,5,9-triphenyl-1,5,9-triphosphacyclododecane;227605-73-4;1,5,9-Triphosphacyclododecane, 1,5,9-triphenyl-;SCHEMBL1531866;DTXSID30436515

Suppliers and Price of 1,5,9-Triphenyl-1,5,9-triphosphacyclododecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5,9-Triphenyl-1,5,9-triphosphacyclododecane

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:450.17951205
Heavy Atom Count:30
Complexity:371

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CP(CCCP(CCCP(C1)C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1,5,9-Triphenyl-1,5,9-triphosphacyclododecane

There total 1 articles about 1,5,9-Triphenyl-1,5,9-triphosphacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7330-49-6
rac-allyl(phenyl)phosphine

: 227605-73-4,287394-83-6
1,5,9-[12]aneP₃Ph₃

Guidance literature:: rac-allyl(phenyl)phosphine; With benzene(cyclopentadienyl)iron(II) hexafluorophosphate; In dichloromethane; Irradiation;

With 2,2'-azobis(isobutyronitrile); In chlorobenzene; at 90 ℃;

With ammonia; sodium; Further stages.;
DOI:10.1039/b002174l

Reference yield: 80.0%

: benzene(cyclopentadienyl)iron(II) hexafluorophosphate

: 227605-73-4,287394-83-6
syn,syn-1,5,9-triphenyl-1,5,9-triphosphacyclododecane

: 287394-81-4
(η5-cyclopentadienyl)(η3-1,5,9-triphenyl-1,5,9-triphosphacyclododecane)iron(II) hexafluorophosphate

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (N2); a soln. of ligand added to a soln. of Fe complex, irradiated with UV for 8 h; evapd. (vac.), recrystd. (MeCN/Et2O);
DOI:10.1039/b509627h

Reference yield: 31.0%

: 10170-68-0,16997-54-9
trichlorotris(tetrahydrofuran)chromium(III)

: 227605-73-4,287394-83-6
1,5,9-[12]aneP₃Ph₃

: 474657-59-5
([12]aneP₃Ph₃)CrCl₃

Guidance literature:: In hexane; dichloromethane; under N2; to a suspn. of Cr complex in CH2Cl2 was added a soln. of the ligand in hexane, the mixt. was stirred for 12 h; the mixt. was filtered, soln. was evapd. in vac., the residue was triturated with hexane, the solid was extd. into warm CH2Cl2, soln. was concd., cooled to -30°C, the solid was filtered, washed with hexane, dried in vac.; elem. anal.;
DOI:10.1039/b203002k