2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)-

Base Information

Chemical Name:2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)-
CAS No.:23632-41-9
Molecular Formula:C10H9BrO
Molecular Weight:225.085
Hs Code.:
Mol file:23632-41-9.mol

Synonyms:(E)-3-(4-bromophenyl)-2-methylacrylate;2-Propenal,3-(4-bromophenyl)-2-methyl-,(2E);

Suppliers and Price of 2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)-

Chemical Property:

PSA：17.07000
LogP:3.05130

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)-

There total 5 articles about 2-Propenal, 3-(4-bromophenyl)-2-methyl-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 123-38-6
propionaldehyde

: 1122-91-4
4-bromo-benzaldehyde

: 23632-41-9
(E)-3-(4-bromophenyl)-2-methylacrylaldehyde

Guidance literature:: With DIMCARB; at 20 ℃; for 48h;
DOI:10.1021/ol047368b

Reference yield:

: (E)-3-(4-bromophenyl)-2-methylprop-2-en-1-ol

: 23632-41-9
(E)-3-(4-bromophenyl)-2-methylacrylaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1002/adsc.202000831

Reference yield:

: 103519-90-0
3-(4-bromophenyl)-2-methylacrylic acid ethyl ester

: 23632-41-9
(E)-3-(4-bromophenyl)-2-methylacrylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

2: Dess-Martin periodane / dichloromethane / 18 h / 20 °C / Inert atmosphere

With diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/adsc.202000831