2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dimethyl ester, (E,E)-

Base Information

Chemical Name:2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dimethyl ester, (E,E)-
CAS No.:23746-55-6
Molecular Formula:C14H14O4
Molecular Weight:246.263
Hs Code.:
Mol file:23746-55-6.mol

Synonyms:1.4-bis-(trans-2-methoxycarbonyl-vinyl)-benzene;dimethyl (2E,2'E)-3,3'-(1,4-phenylene)diprop-2-enoate;methyl p-phenylenediacrylate;(E,E)-1,4-bis-(2-methoxycarbonylvinyl)-benzol;1.4-Bis-(trans-2-methoxycarbonyl-vinyl)-benzol;(2E,2E')-dimethyl 3,3'-(1,4-phenylene)diacrylate;

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Chemical Property of 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dimethyl ester, (E,E)-

Chemical Property:

PSA：52.60000
LogP:2.05900

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dimethyl ester, (E,E)-

There total 11 articles about 2-Propenoic acid, 3,3'-(1,4-phenylene)bis-, dimethyl ester, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 624-38-4,1032416-46-8
para-diiodobenzene

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 23746-55-6
(E)-3-[4-(2-methoxycarbonylvinyl)phenyl]acrylic acid methyl ester

Guidance literature:: With 4Ni⁽²⁺⁾*C₁₈H₁₂N₂O₆^(4-)*2C₃₈H₆₄N₆S₂^(2-)*2ClO₄^(1-)*3H₂O*Pd⁽²⁺⁾; triethylamine; In N,N-dimethyl-formamide; at 130 ℃; for 4h; Inert atmosphere; Schlenk technique;
DOI:10.1002/zaac.201400427

Reference yield: 100.0%

: 23746-55-6
(E)-3-[4-(2-methoxycarbonylvinyl)phenyl]acrylic acid methyl ester

Guidance literature:: With pyridine N-oxide; In dichloromethane; at 23 ℃;
DOI:10.1016/j.jorganchem.2006.05.021

Reference yield: 96.0%

: 106-37-6
1.4-dibromobenzene

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 23746-55-6
(E)-3-[4-(2-methoxycarbonylvinyl)phenyl]acrylic acid methyl ester

Guidance literature:: With potassium carbonate; 1,3-bis(mesityl)imidazolium chloride; palladium diacetate; In N,N-dimethyl-formamide; at 120 ℃; for 60h;
DOI:10.1021/jo800777w