2-Methoxybenzene-1,3-dicarbonyl dichloride

Base Information

Chemical Name:2-Methoxybenzene-1,3-dicarbonyl dichloride
CAS No.:2390-40-1
Molecular Formula:C9H6Cl2O3
Molecular Weight:233.051
Hs Code.:
DSSTox Substance ID:DTXSID50529296
Nikkaji Number:J1.343.013F
Wikidata:Q82399643
Mol file:2390-40-1.mol

Synonyms:2-Methoxyisophthaloyl dichloride;2390-40-1;2-Methoxybenzene-1,3-dicarbonyl dichloride;methoxyisophthaloyl dichloride;SCHEMBL699716;DTXSID50529296;MFCD22055746;SY320675

Suppliers and Price of 2-Methoxybenzene-1,3-dicarbonyl dichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-Methoxybenzene-1,3-dicarbonyl dichloride

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:231.9693994
Heavy Atom Count:14
Complexity:220

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=CC=C1C(=O)Cl)C(=O)Cl

Technology Process of 2-Methoxybenzene-1,3-dicarbonyl dichloride

There total 4 articles about 2-Methoxybenzene-1,3-dicarbonyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004-66-6
2-methoxy-1,3-dimethylbenzene

: 2390-40-1
anisole-2,6-dicarboxylic acid bis acid chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / KMnO₄ / H₂O / 60 °C

2: SOCl₂ / DMF / CH₂Cl₂ / 1.5 h / Heating

With potassium permanganate; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; water;
DOI:10.1002/hlca.200690086

Reference yield:

: 58425-33-5
potassium 2,6-dimethylphenolate

: 2390-40-1
anisole-2,6-dicarboxylic acid bis acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol

2: KOH, K₂MnO₄ / H₂O / 3 h / 80 °C

3: 42 percent / SOCl₂ / Heating

With potassium hydroxide; thionyl chloride; potassium permanganate; In methanol; water;
DOI:10.1021/ja00169a031

Reference yield:

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 2390-40-1
anisole-2,6-dicarboxylic acid bis acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / KOH / dimethylsulfoxide / 0.25 h / 0 - 20 °C

2: 52 percent / KMnO₄ / H₂O / 60 °C

3: SOCl₂ / DMF / CH₂Cl₂ / 1.5 h / Heating

With potassium hydroxide; potassium permanganate; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/hlca.200690086