Benzenesulfonamide, 2,6-dimethyl- (9CI)

Base Information

• Chemical Name: Benzenesulfonamide, 2,6-dimethyl- (9CI)
• CAS No.: 24010-56-8
• Molecular Formula: C8H11NO2S
• Molecular Weight: 185.247
• Hs Code.: 2935009090
• Mol file: 24010-56-8.mol

Synonyms:2,6-dimethyl-benzenesulfonic acid amide;2,6-Dimethyl-benzolsulfonsaeure-amid;2,6-Dimethylbenzolsulfonamid;Benzenesulfonamide,2,6-dimethyl;

Chemical Property of Benzenesulfonamide, 2,6-dimethyl- (9CI)

Chemical Property:

• Vapor Pressure: 6.66E-05mmHg at 25°C
• Melting Point: 112-113 °C
• Boiling Point: 344.3oC at 760 mmHg
• PKA: 10.27±0.60(Predicted)
• Flash Point: 162oC
• PSA: 68.54000
• Density: 1.227g/cm3
• LogP: 2.73190

Purity/Quality:

99% ^*data from raw suppliers

2,6-DIMETHYL-BENZENESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, 2,6-dimethyl- (9CI)

There total 3 articles about Benzenesulfonamide, 2,6-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dimethyl-benzene-sulfonyl chloride (2905-29-5) → 2,6-dimethylbenzenesulfonamide (24010-56-8)

Guidance literature:

With ammonium hydroxide; In acetonitrile; at 0 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1016/j.bmcl.2014.02.054

Reference yield:

hydrogen sulfide (7783-06-4) + ammonium hydroxide + 2,6-dimethylaniline (87-62-7) → 2,6-dimethylbenzenesulfonamide (24010-56-8)

Guidance literature:

With hydrogenchloride; sodium sulfide; sodium nitrite; In chloroform; water; acetic acid; sodium disulfide;

Reference yield:

→ 2,6-dimethylbenzenesulfonamide (24010-56-8)

Guidance literature:

entspr. S.;

DOI:10.1021/jo00831a084

upstream raw materials:

hydrogen sulfide

2,6-dimethylaniline

2,6-dimethyl-benzene-sulfonyl chloride

Downstream raw materials:

2,2'-dithiobis<3-methylbenzoic acid>

Refernces

• 1、 -. "Herbicidal compounds, their production and use". . . Retrieved 2008/06/13.