Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester
CAS No.:24629-99-0
Molecular Formula:C16H17N3O2
Molecular Weight:283.33
Hs Code.:
DSSTox Substance ID:DTXSID201040914

Synonyms:24629-99-0;DTXSID201040914;Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester

Suppliers and Price of Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:283.132076794
Heavy Atom Count:21
Complexity:363

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)N=NC2=CC=CC(=C2)C(=O)OC

Technology Process of Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester

There total 2 articles about Benzoic acid, 3-[2-[4-(dimethylamino)phenyl]diazenyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4518-10-9
Methyl 3-aminobenzoate

: 121-69-7,77733-26-7
N,N-dimethyl-aniline

: 24629-99-0
methyl 3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoate

Guidance literature:: Methyl 3-aminobenzoate; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.5h;

N,N-dimethyl-aniline; In water; at 0 ℃; for 1h;

With sodium hydrogencarbonate; In water; Cooling with ice;
DOI:10.1002/anie.201109265

Reference yield:

: 24629-99-0
methyl 3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoate

Guidance literature:: Dimethylanilin, entspr. diazot. subst. Anilin;

Reference yield: 97.0%

: 24629-99-0
methyl 3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoate

: 35282-69-0
(3-((4-(dimethylamino)phenyl)diazenyl)phenyl)methanol

Guidance literature:: methyl 3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; Cooling with ice;
DOI:10.1002/anie.201109265