4-Hydroxymethyl-4-methyl-cyclohex-2-enone

Base Information

Chemical Name:4-Hydroxymethyl-4-methyl-cyclohex-2-enone
CAS No.:24730-93-6
Molecular Formula:C8H12O2
Molecular Weight:140.18000
Hs Code.:2914400090
DSSTox Substance ID:DTXSID10442972
Nikkaji Number:J895.420H
Mol file:24730-93-6.mol

Synonyms:4-HYDROXYMETHYL-4-METHYL-CYCLOHEX-2-ENONE;24730-93-6;4-(HYDROXYMETHYL)-4-METHYLCYCLOHEX-2-EN-1-ONE;DTXSID10442972;AKOS006331118;4-Methyl-4-(hydroxymethyl)-2-cyclohexen-1-one

Suppliers and Price of 4-Hydroxymethyl-4-methyl-cyclohex-2-enone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-HYDROXYMETHYL-4-METHYL-CYCLOHEX-2-ENONE 95.00%
5MG
$ 502.83

Total 4 raw suppliers

Chemical Property of 4-Hydroxymethyl-4-methyl-cyclohex-2-enone

Chemical Property:

PSA：37.30000
LogP:0.90410
XLogP3:0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:140.083729621
Heavy Atom Count:10
Complexity:172

Purity/Quality:

99% ^*data from raw suppliers

4-HYDROXYMETHYL-4-METHYL-CYCLOHEX-2-ENONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCC(=O)C=C1)CO

Technology Process of 4-Hydroxymethyl-4-methyl-cyclohex-2-enone

There total 9 articles about 4-Hydroxymethyl-4-methyl-cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: [(1S,2R)-4-(tert-Butyl-dimethyl-silanyloxy)-2-dimethylamino-1-methyl-cyclohex-3-enyl]-methanol

: 24730-93-6
4-(hydroxymethyl)-4-methyl-2-cyclohexene-1-one

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; water; at 5 - 20 ℃; for 20h;
DOI:10.15227/orgsyn.078.0160

Reference yield: 80.0%

: 1-(tert-butyldimethylsilyloxy)-4-formyl-4-methyl-3-(2-oxazolidinon-3-yl)cyclohexene

: 24730-93-6
4-(hydroxymethyl)-4-methyl-2-cyclohexene-1-one

Guidance literature:: 1-(tert-butyldimethylsilyloxy)-4-formyl-4-methyl-3-(2-oxazolidinon-3-yl)cyclohexene; With lithium aluminium tetrahydride; In diethyl ether; at -78 - 20 ℃; for 96h;

With hydrogen fluoride; In acetonitrile; at 20 ℃; for 2.5h; Further stages.;
DOI:10.1021/jo005619y

Reference yield: 61.0%

: C₁₂H₁₈O₄

: 24730-93-6
4-(hydroxymethyl)-4-methyl-2-cyclohexene-1-one

Guidance literature:: C₁₂H₁₈O₄; With lithium aluminium tetrahydride; In diethyl ether; at 0 - 23 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; In diethyl ether; water; at 23 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/jo502809d