1,2-Hydrazinedicarboxylic acid, 1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:1,2-Hydrazinedicarboxylic acid, 1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester
CAS No.:250665-92-0
Molecular Formula:C30H43N3O8
Molecular Weight:573.687
Hs Code.:

1,2-Hydrazinedicarboxylic acid,
1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen
ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester

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Chemical Property of 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester

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Technology Process of 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester

There total 3 articles about 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-1-(3,4-dimethoxyphenyl)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phen ylethyl]methylamino]-2-oxoethyl]-, bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 870-50-8
(Z)-N-[(tert-butoxy)carbonyl]imino(tert-butoxy)formamide

: 234089-44-2
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide

: 250665-92-0
[2S,1'S,2'S]-(+)-2-(3,4-dimethoxyphenyl)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methylacetamide

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

(Z)-N-[(tert-butoxy)carbonyl]imino(tert-butoxy)formamide; In tetrahydrofuran; at -105 ℃;
DOI:10.1016/S0040-4039(99)01475-6

Reference yield: 89.0%

: 16466-61-8
1,2-bis(t-butyloxycarbonyl)hydrazine

: 234089-44-2
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide

: 250665-92-0
[2S,1'S,2'S]-(+)-2-(3,4-dimethoxyphenyl)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methylacetamide

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.33333h;

1,2-bis(t-butyloxycarbonyl)hydrazine; In tetrahydrofuran; hexane; at -105 ℃; for 1h;
DOI:10.1002/1099-0690(200111)2001:22<4343::AID-EJOC4343>3.0.CO;2-D

Reference yield: 89.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 234089-44-2
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide

: 250665-92-0
[2S,1'S,2'S]-(+)-2-(3,4-dimethoxyphenyl)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methylacetamide

: C₃₀H₄₃N₃O₈

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-2-(3,4-dimethoxyphenyl)-N-methylacetamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; at -105 ℃;
DOI:10.1016/S0957-4166(02)00181-7