1,2-Hydrazinedicarboxylic acid, 1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:1,2-Hydrazinedicarboxylic acid, 1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester
CAS No.:250665-95-3
Molecular Formula:C31H45N3O9
Molecular Weight:603.713
Hs Code.:

1,2-Hydrazinedicarboxylic acid,
1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox
o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester

Synonyms:

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Chemical Property of 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester

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Technology Process of 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester

There total 3 articles about 1,2-Hydrazinedicarboxylic acid, 1-[(1S)-2-[[(1S,2S)-2-hydroxy-1-methyl-2-phenylethyl]methylamino]-2-ox o-1-(3,4,5-trimethoxyphenyl)ethyl]-, bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 870-50-8
(Z)-N-[(tert-butoxy)carbonyl]imino(tert-butoxy)formamide

: 247118-51-0
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

: 250665-95-3
[2S,1'S,2'S]-(+)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

(Z)-N-[(tert-butoxy)carbonyl]imino(tert-butoxy)formamide; In tetrahydrofuran; at -105 ℃;
DOI:10.1016/S0040-4039(99)01475-6

Reference yield: 90.0%

: 16466-61-8
1,2-bis(t-butyloxycarbonyl)hydrazine

: 247118-51-0
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

: 250665-95-3
[2S,1'S,2'S]-(+)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.33333h;

1,2-bis(t-butyloxycarbonyl)hydrazine; In tetrahydrofuran; hexane; at -105 ℃; for 1h;
DOI:10.1002/1099-0690(200111)2001:22<4343::AID-EJOC4343>3.0.CO;2-D

Reference yield: 90.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 247118-51-0
(+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

: 250665-95-3
[2S,1'S,2'S]-(+)-2-[N,N'-bis(1,1-dimethylethoxycarbonyl)hydrazino]-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide

: C₃₁H₄₅N₃O₉

Guidance literature:: (+)-<1'S,2'S>-N-(2'-hydroxy-1'-methyl-2'-phenylethyl)-N-methyl-2-(3,4,5-trimethoxyphenyl)acetamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; at -105 ℃;
DOI:10.1016/S0957-4166(02)00181-7