Benzoic acid, 2-(diphenylarsino)-

Base Information

Chemical Name:Benzoic acid, 2-(diphenylarsino)-
CAS No.:25334-69-4
Molecular Formula:C19H15AsO2
Molecular Weight:350.248
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 2-(diphenylarsino)-

Chemical Property:

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Technology Process of Benzoic acid, 2-(diphenylarsino)-

There total 7 articles about Benzoic acid, 2-(diphenylarsino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 111382-65-1
methyl 2-(diphenylarsino)benzoate

: 25334-69-4
o-(diphenylarsino)bensoic acid

Guidance literature:: methyl 2-(diphenylarsino)benzoate; With potassium tert-butylate; In diethyl ether; at 0 - 20 ℃;

With hydrogenchloride; In water; Cooling with ice;
DOI:10.1021/om400144s

Reference yield:

: 603-32-7
triphenyl-arsane

: 25334-69-4
o-(diphenylarsino)bensoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia; sodium / Inert atmosphere; Cooling with ethanol-dry ice

1.2: 0.08 h / Inert atmosphere; Cooling with ethanol-dry ice

2.1: bis-triphenylphosphine-palladium(II) chloride / toluene / 24 h / 100 °C / Inert atmosphere

3.1: potassium tert-butylate / diethyl ether / 0 - 20 °C

3.2: Cooling with ice

With bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; ammonia; sodium; In diethyl ether; toluene;
DOI:10.1021/om400144s

Reference yield:

: 101319-72-6
n-Bu₃SnAsPh₂

: 25334-69-4
o-(diphenylarsino)bensoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium chloride; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / N,N-dimethyl-formamide / 24 h / 120 °C / Inert atmosphere

2.1: potassium tert-butylate / diethyl ether / 0 - 20 °C

2.2: Cooling with ice

With bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; triphenylphosphine; lithium chloride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/om400144s