1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone

Base Information

Chemical Name:1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone
CAS No.:25892-94-8
Molecular Formula:C16H16O5
Molecular Weight:288.3
Hs Code.:2914509090
Mol file:25892-94-8.mol

Synonyms:4-Benzyloxy-2,5-dihydroxy-6-methoxyacetophenon;4-benzyloxy-2,5-dihydroxy-6-methoxyacetophenone;1-(4-Benzyloxy-3,6-dihydroxy-2-methoxy-phenyl)-aethanon;Ethanone,1-[3,6-dihydroxy-2-methoxy-4-(phenylmethoxy)phenyl];1-(4-benzyloxy-3,6-dihydroxy-2-methoxy-phenyl)-ethanone;

Suppliers and Price of 1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(4-(Benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethanone 95+%
1g
$ 491.00

Alichem
1-(4-(Benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethanone
1g
$ 998.00

AK Scientific
1-(4-(Benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethanone
1g
$ 1680.00

Total 12 raw suppliers

Chemical Property of 1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone

Chemical Property:

Melting Point:161-162 °C
Boiling Point:517.6±50.0 °C(Predicted)
PKA:9.37±0.50(Predicted)
PSA：75.99000
Density:1.272±0.06 g/cm3(Predicted)
LogP:2.88800
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

1-(4-(Benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone

There total 11 articles about 1-(4-(benzyloxy)-3,6-dihydroxy-2-Methoxyphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

concentrated hydrogen chloride: concentrated hydrogen chloride

: 39548-89-5
1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethan-1-one

: 77-98-5
tetraethylammonium hydroxide

: 25892-94-8
1-(4-(benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethan-1-one

Guidance literature:: With pyridine; hydrogenchloride; dipotassium peroxodisulfate; sodium sulfite; In water; benzene;

Reference yield: 31.0%

: 39548-89-5
1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethan-1-one

: 25892-94-8
1-(4-(benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethan-1-one

Guidance literature:: 1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethan-1-one; With pyridine; tetraethylammonium hydroxide; In water; at 20 ℃;

With dipotassium peroxodisulfate; In water; at 20 ℃; for 24h;

With hydrogenchloride; sodium sulfite; In water; benzene; at 95 ℃; for 1h;

Reference yield:

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 25892-94-8
1-(4-(benzyloxy)-3,6-dihydroxy-2-methoxyphenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / aluminium chloride / chlorobenzene / 1 h / Heating

2: 99 percent / K₂CO₃ / acetone / Heating

3: 29 percent / NaOH; K₂S₂O₈; pyridine / H₂O / 24 h / 20 °C

With pyridine; sodium hydroxide; dipotassium peroxodisulfate; aluminium trichloride; potassium carbonate; In water; chlorobenzene; acetone; 3: Elbs persulfate oxidation;
DOI:10.1038/sj.bjp.0705828