4-(1-(Diphenylmethyl)butyl)-1H-imidazole

Base Information

• Chemical Name: 4-(1-(Diphenylmethyl)butyl)-1H-imidazole
• CAS No.: 106147-70-0
• Molecular Formula: C20H22 N2
• Molecular Weight: 290.408
• DSSTox Substance ID: DTXSID50909938
• Mol file: 106147-70-0.mol

Synonyms:BRN 4194226;4-(1-(Diphenylmethyl)butyl)-1H-imidazole;4(5)-(2-(1,1-Diphenyl)-pentyl)imidazole;1H-Imidazole, 4-(1-(diphenylmethyl)butyl)-;106147-70-0;5-(1,1-diphenylpentan-2-yl)-1H-imidazole;DTXSID50909938;LS-78539

Chemical Property of 4-(1-(Diphenylmethyl)butyl)-1H-imidazole

Chemical Property:

• Vapor Pressure: 2.29E-07mmHg at 25°C
• Boiling Point: 435.1°Cat760mmHg
• Flash Point: 209.2°C
• Density: 1.081g/cm³
• XLogP3: 5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 6
• Exact Mass: 290.178298710
• Heavy Atom Count: 22
• Complexity: 287

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC(C1=CN=CN1)C(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 4-(1-(Diphenylmethyl)butyl)-1H-imidazole

There total 5 articles about 4-(1-(Diphenylmethyl)butyl)-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4(5)-<(2,2-diphenyl-1-n-propyl)-ethenyl>imidazole (106147-69-7) → 4(5)-<2-(1,1-diphenyl)-pentyl>imidazole (106147-70-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 70 ℃; for 6h; under 2040.2 Torr;

DOI:10.1016/0223-5234(90)90180-B

Reference yield:

Diphenylmethane (101-81-5) → 4(5)-<2-(1,1-diphenyl)-pentyl>imidazole (106147-70-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) hexane, THF, 0 deg C, 2.) RT, 2 h

2: 67 percent / 90percent acetic acid / 1 h / Heating

3: 83 percent / H₂ / 10percent Pd/C / ethanol / 6 h / 70 °C / 2040.2 Torr

With n-butyllithium; hydrogen; acetic acid; palladium on activated charcoal; In ethanol;

DOI:10.1016/0223-5234(90)90180-B

Reference yield:

4-butanoyl-1-tritylimidazole (132303-12-9) → 4(5)-<2-(1,1-diphenyl)-pentyl>imidazole (106147-70-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) hexane, THF, 0 deg C, 2.) RT, 2 h

2: 67 percent / 90percent acetic acid / 1 h / Heating

3: 83 percent / H₂ / 10percent Pd/C / ethanol / 6 h / 70 °C / 2040.2 Torr

With n-butyllithium; hydrogen; acetic acid; palladium on activated charcoal; In ethanol;

DOI:10.1016/0223-5234(90)90180-B

upstream raw materials:

4(5)-<(2,2-diphenyl-1-n-propyl)-ethenyl>imidazole

Diphenylmethane

4-butanoyl-1-tritylimidazole

4-<2-(1,1-diphenyl-2-hydroxy)-pentyl>-1-tritylimidazole