diethyl nona-2,7-dienedioate

Base Information

• Chemical Name: diethyl nona-2,7-dienedioate
• CAS No.: 26385-65-9
• Molecular Formula: C13H20O4
• Molecular Weight: 240.299

Synonyms:

Chemical Property of diethyl nona-2,7-dienedioate

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diethyl nona-2,7-dienedioate

There total 2 articles about diethyl nona-2,7-dienedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1 ,5-pentanediol (111-29-5) + ethyl (triphenylphosphoranylidene)acetate (1099-45-2) → 3,4,5,6-tetrahydro-2H-pyran-2-one (542-28-9,26354-94-9) + nona-2,7-dienedioic acid diethyl ester (26385-65-9) + (Z)-7-hydroxy-hept-2-enoic acid ethyl ester (105198-41-2) + ethyl (E)-7-hydroxyhept-2-enoate (96251-91-1)

Guidance literature:

With manganese(IV) oxide; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2007.07.089

Reference yield:

diethyl nona-2,7-diynedioate (34497-18-2) → nona-2c,7c-dienedioic acid diethyl ester (15898-67-6,15898-68-7,26385-65-9)

Guidance literature:

With Lindlar's catalyst; ethanol; Hydrogenation;

Reference yield: 26.0%

nona-2,7-dienedioic acid diethyl ester (26385-65-9) + trifluoroacetic acid (76-05-1) → 2-(1-Ethoxycarbonyl-2,2,2-trifluoro-ethyl)-6-trifluoromethyl-cyclohexanecarboxylic acid ethyl ester

Guidance literature:

With sodium hydroxide; In ethanol; water; acetonitrile; at 22 ℃; for 7h; electrolysis, 1.8 A;

DOI:10.1139/v82-229

upstream raw materials:

diethyl nona-2,7-diynedioate

1 ,5-pentanediol

ethyl (triphenylphosphoranylidene)acetate

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