tricyclo[3.2.1.0~3,6~]octane

Base Information

Chemical Name:tricyclo[3.2.1.0~3,6~]octane
CAS No.:250-22-6
Molecular Formula:C₈H₁₂
Molecular Weight:108.183
Hs Code.:
Mol file:250-22-6.mol

Synonyms:Tricyclo<3.2.1.03.6>octan;tricyclo<3.2.1.03,6>octane;

Suppliers and Price of tricyclo[3.2.1.0~3,6~]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of tricyclo[3.2.1.0~3,6~]octane

Chemical Property:

Vapor Pressure:9.08mmHg at 25°C
Melting Point:110-112 °C(bomb tube)
Boiling Point:136.6°Cat760mmHg
Flash Point:14.1°C
PSA：0.00000
Density:1.04g/cm³
LogP:2.05240

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tricyclo[3.2.1.0~3,6~]octane

There total 12 articles about tricyclo[3.2.1.0~3,6~]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 79647-59-9
tert-butyl tricyclo<3.2.1.0^3,6>octane-1-percarboxylate

: 250-22-6
Tricyclo<3.2.1.0^3,6>octan

Guidance literature:: In various solvent(s); for 1h; Heating;
DOI:10.1021/jo00339a013

Reference yield:

: (1R,2R,4S,5S,6R)-6-Chloromethyl-3-oxa-tricyclo[3.2.1.0^2,4]octane

: 250-22-6
Tricyclo<3.2.1.0^3,6>octan

Guidance literature:: Multi-step reaction with 3 steps

1: Li, BF₃*Et₂O / tetrahydrofuran

2: K₂Cr₂O₇, aq. H₂SO₄

3: (i) N₂H₄*H₂O, AcOH, (ii) NaOMe, MeOH

With potassium dichromate; sulfuric acid; boron trifluoride diethyl etherate; lithium; In tetrahydrofuran;
DOI:10.1021/ja00962a032

Reference yield:

: 6239-89-0,6239-90-3,87507-42-4,87507-44-6,87507-45-7,87507-60-6,87507-61-7,90528-09-9
exo-Tricyclo<3.2.1.0^3.6>octanol-2

: 250-22-6
Tricyclo<3.2.1.0^3,6>octan

Guidance literature:: Multi-step reaction with 2 steps

1: K₂Cr₂O₇, aq. H₂SO₄

2: (i) N₂H₄*H₂O, AcOH, (ii) NaOMe, MeOH

With potassium dichromate; sulfuric acid;
DOI:10.1021/ja00962a032