4-(3-Bromobenzo[b]thien-2-yl)phenol

Base Information

Chemical Name:4-(3-Bromobenzo[b]thien-2-yl)phenol
CAS No.:265654-84-0
Molecular Formula:C14H9BrOS
Molecular Weight:305.195
Hs Code.:
DSSTox Substance ID:DTXSID601293444
Nikkaji Number:J2.408.812J

Synonyms:SCHEMBL7352370;KDFBIIKWAQLQGQ-UHFFFAOYSA-N;DTXSID601293444;4-(3-Bromobenzo[b]thien-2-yl)phenol;265654-84-0;3-bromo-2-(4-hydroxyphenyl)benzo[b]-thiophene

Suppliers and Price of 4-(3-Bromobenzo[b]thien-2-yl)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-(3-Bromobenzo[b]thien-2-yl)phenol

Chemical Property:

XLogP3:4.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:303.95575
Heavy Atom Count:17
Complexity:265

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=C(S2)C3=CC=C(C=C3)O)Br

Technology Process of 4-(3-Bromobenzo[b]thien-2-yl)phenol

There total 4 articles about 4-(3-Bromobenzo[b]thien-2-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 924633-97-6
o-(4-hydroxyphenylethynyl)thioanisole

: 265654-84-0
2-(4-hydroxyphenyl)-3-bromobenzo[b]thiophene

Guidance literature:: With copper(ll) bromide; In acetonitrile; Heating;
DOI:10.1016/j.tet.2006.10.068

Reference yield:

: 2200-91-1
4-ethynylphenol

: 265654-84-0
2-(4-hydroxyphenyl)-3-bromobenzo[b]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: CuI; n-BuNH₂ / Pd(PPh₃)4 / diethyl ether / 4 h / 20 °C

2: 81 percent / CuBr₂ / acetonitrile / Heating

With copper(l) iodide; N-butylamine; copper(ll) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; acetonitrile; 1: Sonogashira coupling;
DOI:10.1016/j.tet.2006.10.068

Reference yield:

: 33775-94-9
2-(methylthio)iodobenzene

: 265654-84-0
2-(4-hydroxyphenyl)-3-bromobenzo[b]thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: CuI; n-BuNH₂ / Pd(PPh₃)4 / diethyl ether / 4 h / 20 °C

2: 81 percent / CuBr₂ / acetonitrile / Heating

With copper(l) iodide; N-butylamine; copper(ll) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In diethyl ether; acetonitrile; 1: Sonogashira coupling;
DOI:10.1016/j.tet.2006.10.068