Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-

Base Information

Chemical Name:Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-
CAS No.:26592-77-8
Molecular Formula:C18H16
Molecular Weight:232.325
Hs Code.:
DSSTox Substance ID:DTXSID50372926
Nikkaji Number:J690.628A
Wikidata:Q82160921

Synonyms:Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-;5,5-diphenylcyclohexadiene;26592-77-8;DTXSID50372926;5,5-Diphenyl-1,3-cyclohexadiene;AKOS004907518

Suppliers and Price of Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(1-PHENYLCYCLOHEXA-2,4-DIEN-1-YL)BENZENE 95.00%
5MG
$ 495.96

Total 1 raw suppliers

Chemical Property of Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-

Chemical Property:

PSA：0.00000
LogP:4.48880
XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:232.125200510
Heavy Atom Count:18
Complexity:293

Purity/Quality:

99% ^*data from raw suppliers

(1-PHENYLCYCLOHEXA-2,4-DIEN-1-YL)BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1C=CC=CC1(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis-

There total 6 articles about Benzene, 1,1'-(2,4-cyclohexadien-1-ylidene)bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 123994-44-5
5,5-diphenyl-2-{[(trifluoromethyl)sulfonyl]oxy}-1,3-cyclohexadiene

: 26592-77-8
5,5-diphenyl-1,3-cyclohexadiene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimethylamine borane; potassium carbonate; In acetonitrile; at 40 ℃; for 1.25h;
DOI:10.1016/S0040-4039(99)01255-1

Reference yield:

: 21195-66-4
4,4-diphenyl-2-cyclohexenone tosylhydrazone

: 26592-77-8
5,5-diphenyl-1,3-cyclohexadiene

Guidance literature:: With n-butyllithium;
DOI:10.1021/ja00780a019

Reference yield:

: 4528-64-7
4,4-diphenyl-2-cyclohexen-1-one

: 26592-77-8
5,5-diphenyl-1,3-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-lutidine / CH₂Cl₂ / 20 °C

2: 81 percent / dimethylamine*borane complex; Pd(PPh₃)4; K₂CO₃ / acetonitrile / 1.25 h / 40 °C

With 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dimethylamine borane; potassium carbonate; In dichloromethane; acetonitrile; 1: triflation / 2: Reduction;
DOI:10.1016/S0040-4039(99)01255-1