2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

Base Information

Chemical Name:2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide
CAS No.:27285-13-8
Molecular Formula:C16H17N3O2S
Molecular Weight:315.39000
Hs Code.:
Mol file:27285-13-8.mol

Synonyms:2-(N'-Phenylureido)-4.5.6.7-tetrahydrobenzo[b]thiophensaeureamid;

Suppliers and Price of 2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Aronis compounds
2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide
1mg
$ 12.00

Total 0 raw suppliers

Chemical Property of 2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

Chemical Property:

PSA：112.46000
LogP:4.21610

Purity/Quality:: 2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide

There total 3 articles about 2-[(anilinocarbonyl)amino]-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 103-71-9
phenyl isocyanate

: 4815-28-5
2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxamide

: 27285-13-8
2-(3-phenylurea)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxamide

Guidance literature:: In dichloromethane; for 120h; Reflux;

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 27285-13-8
2-(3-phenylurea)-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol

2: diethylamine; sulfur / 3 h / 50 °C

3: dichloromethane / 120 h / Reflux

With sulfur; diethylamine; In ethanol; dichloromethane;