Technology Process of 2-Furanoctanoic acid
There total 1 articles about 2-Furanoctanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: sodium ethylate; ethanol / anschliessendes Erwaermen mit 6-Brom-hexansaeure-aethylester in Benzol
2: aqueous KOH-solution / Erhitzen des Reaktionsprodukts mit wss. Schwefelsaeure
3: hydrazine hydrate; sodium hydroxide; ethylene glycol / 150 °C / Entfernen des entstehenden Wassers und Erhitzen des Reaktionsprodukts mit Toluol und wss.-aethanol. Natronlauge
With
potassium hydroxide; sodium hydroxide; ethanol; sodium ethanolate; hydrazine hydrate; ethylene glycol;
- Guidance literature:
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Multi-step reaction with 3 steps
1.1: sodium dihydrogenphosphate; sodium chlorite / water; tert-butyl alcohol / 1.5 h / 20 °C
2.1: sodium tetrahydroborate / methanol / 20 °C / Cooling with ice
2.2: 0.5 h / 20 °C / pH 3
3.1: N-ethyl-N,N-diisopropylamine / acetonitrile / 2 h / 20 °C
With
sodium chlorite; sodium tetrahydroborate; sodium dihydrogenphosphate; N-ethyl-N,N-diisopropylamine;
In
methanol; water; acetonitrile; tert-butyl alcohol;
DOI:10.1021/tx200093m
- Guidance literature:
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Multi-step reaction with 3 steps
1: benzene; sulfuric acid
2: boron fluoride ether adduct
3: aqueous acetic acid
With
boron fluoride ether; sulfuric acid; acetic acid; benzene;
