4-(hexyloxy)-3-nitrobenzoic acid

Base Information

• Chemical Name: 4-(hexyloxy)-3-nitrobenzoic acid
• CAS No.: 281195-35-5
• Molecular Formula: C₁₃H₁₇NO₅
• Molecular Weight: 267.282
• Mol file: 281195-35-5.mol

Synonyms:4-hexyloxy-3-nitro benzoic acid;Benzoic acid,4-(hexyloxy)-3-nitro;

Chemical Property of 4-(hexyloxy)-3-nitrobenzoic acid

Chemical Property:

• PSA: 92.35000
• LogP: 3.77530

Purity/Quality:

4-Hexyloxy-3-nitrobenzoic acid 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(hexyloxy)-3-nitrobenzoic acid

There total 4 articles about 4-(hexyloxy)-3-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hexyloxy-3-nitro benzoic acid ethyl ester → 4-hexyloxy-3-nitro benzoic acid (281195-35-5)

Guidance literature:

With sodium hydroxide; In ethanol;

Reference yield:

ethyl 4-hydroxy-3-nitrobenzoate (19013-10-6) → 4-hexyloxy-3-nitro benzoic acid (281195-35-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃; KI / dimethylformamide

2: aq. NaOH / ethanol

With sodium hydroxide; potassium carbonate; potassium iodide; In ethanol; N,N-dimethyl-formamide;

Reference yield:

3-nitro-4-hydroxybenzoic acid (616-82-0) → 4-hexyloxy-3-nitro benzoic acid (281195-35-5)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄

2: K₂CO₃; KI / dimethylformamide

3: aq. NaOH / ethanol

With sodium hydroxide; sulfuric acid; potassium carbonate; potassium iodide; In ethanol; N,N-dimethyl-formamide;

upstream raw materials:

ethyl 4-hydroxy-3-nitrobenzoate

3-nitro-4-hydroxybenzoic acid