1-{1-(2-phenylethyl)-3-[(phenylsulfanyl)methyl]triaz-2-en-1-yl}ethanone

Base Information

• Chemical Name: 1-{1-(2-phenylethyl)-3-[(phenylsulfanyl)methyl]triaz-2-en-1-yl}ethanone
• CAS No.: 84304-09-6
• Molecular Formula: C17H19 N3 O S
• Molecular Weight: 313.423

Synonyms:1-Triazene,3-acetyl-3-(2-phenylethyl)-1-[(phenylthio)methyl]- (9CI); NSC 370655

Chemical Property of 1-{1-(2-phenylethyl)-3-[(phenylsulfanyl)methyl]triaz-2-en-1-yl}ethanone

Chemical Property:

• Vapor Pressure: 1.06E-07mmHg at 25°C
• Boiling Point: 433°Cat760mmHg
• Flash Point: 215.7°C
• Density: 1.11g/cm³

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of 1-{1-(2-phenylethyl)-3-[(phenylsulfanyl)methyl]triaz-2-en-1-yl}ethanone

There total 1 articles about 1-{1-(2-phenylethyl)-3-[(phenylsulfanyl)methyl]triaz-2-en-1-yl}ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenethylmagnesium bromide (3277-89-2) + azidomethyl phenyl sulphide (77422-70-9) + acetic anhydride (108-24-7) → C17H19N3OS (84304-09-6)

Guidance literature:

Yield given. Multistep reaction; 1.) -78 deg C, 2.) -78 deg C;

DOI:10.1021/ja00342a069

Reference yield: 70.0%

C17H19N3OS (84304-09-6) → methyl-N-(benzyl-methyl)-formamide (877-95-2)

Guidance literature:

With tetra(n-butyl)ammonium formate; In N,N-dimethyl-formamide; at 45 ℃;

DOI:10.1021/ja00342a069

upstream raw materials:

phenethylmagnesium bromide

azidomethyl phenyl sulphide

acetic anhydride

Downstream raw materials:

methyl-N-(benzyl-methyl)-formamide

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