Methanone, bis[4-(4-bromobutoxy)phenyl]-

Base Information

• Chemical Name: Methanone, bis[4-(4-bromobutoxy)phenyl]-
• CAS No.: 288248-48-6
• Molecular Formula: C21H24Br2O3
• Molecular Weight: 484.228
• DSSTox Substance ID: DTXSID00478745
• Mol file: 288248-48-6.mol

Synonyms:Methanone, bis[4-(4-bromobutoxy)phenyl]-;288248-48-6;DTXSID00478745

Chemical Property of Methanone, bis[4-(4-bromobutoxy)phenyl]-

Chemical Property:

• XLogP3: 6.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 12
• Exact Mass: 484.00717
• Heavy Atom Count: 26
• Complexity: 342

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)C2=CC=C(C=C2)OCCCCBr)OCCCCBr

Technology Process of Methanone, bis[4-(4-bromobutoxy)phenyl]-

There total 2 articles about Methanone, bis[4-(4-bromobutoxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.6%

1,4-dibromo-butane (110-52-1) + 4,4'-Dihydroxybenzophenone (611-99-4) → 4,4'-di(4-bromo-1-butoxy)benzophenone (288248-48-6)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; at 60 ℃; for 12h;

DOI:10.1039/c7cc01093a

Reference yield:

1,4-dibromo-butane (110-52-1) + 4-Hydroxybenzophenone (1137-42-4) → 4,4'-di(4-bromo-1-butoxy)benzophenone (288248-48-6)

Guidance literature:

4-Hydroxybenzophenone; With sodium hydroxide; In ethanol; at 20 ℃; for 0.5h;

1,4-dibromo-butane; In ethanol; at 85 ℃; for 24h;

DOI:10.1002/chem.201904443

Reference yield: 47.2%

4,4'-di(4-bromo-1-butoxy)benzophenone (288248-48-6) → 1, 1, 2, 2-tetrakis(4-(4-bromobutoxy)phenyl)ethylene (1204389-23-0)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran; at -78 - 85 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.tetlet.2014.01.062

upstream raw materials:

1,4-dibromo-butane

4,4'-Dihydroxybenzophenone

4-Hydroxybenzophenone

Downstream raw materials:

1, 1, 2, 2-tetrakis(4-(4-bromobutoxy)phenyl)ethylene