CID 18927055

Base Information

• Chemical Name: CID 18927055
• CAS No.: 28902-93-4
• Molecular Formula: C6H14N2O3
• Molecular Weight: 162.18700
• DSSTox Substance ID: DTXSID10951534
• Mol file: 28902-93-4.mol

Synonyms:28902-93-4;N~2~-Hydroxylysine;SCHEMBL48406;DTXSID10951534;6-amino-2-(hydroxyamino)hexanoic acid

Chemical Property of CID 18927055

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 369.614oC at 760 mmHg
• PKA: pK1:2.13(＋2);pK2:8.62(＋1);pK3:9.67(0) (38°C,μ=0.1)
• Flash Point: 177.336oC
• PSA: 95.58000
• Density: 1.223g/cm3
• LogP: 0.63860
• XLogP3: -3.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 6
• Exact Mass: 162.10044231
• Heavy Atom Count: 11
• Complexity: 118

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CCN)CC(C(=O)O)NO

Technology Process of CID 18927055

There total 74 articles about CID 18927055 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(2S,5R)-2,6-diazido-5-hydroxyhexanoic acid → (5R)-5-hydroxy-L-lysine (504-91-6,1190-94-9,3506-26-1,6000-08-4,18899-29-1,18899-30-4,18899-31-5,52153-41-0,78088-29-6,28902-93-4)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; at 20 ℃; for 15h; under 760.051 Torr;

DOI:10.1039/c4ob01220h

Reference yield:

L-lysine (56-87-1,3506-25-0) → (2S,5S)-5-hydroxylysine (18899-29-1,28902-93-4) + (5R)-5-hydroxy-L-lysine (504-91-6,1190-94-9,3506-26-1,6000-08-4,18899-29-1,18899-30-4,18899-31-5,52153-41-0,78088-29-6,28902-93-4) + (2S)-4-hydroxylysine (15574-69-3) + (2S)-2,6-diamino-3-hydroxyhexanoic acid

Guidance literature:

With oxygen; In water; γ-Irradiation;

DOI:10.1021/tx980118h

Reference yield:

L-lysine (56-87-1,3506-25-0) → (2S,5S)-5-hydroxylysine (18899-29-1,28902-93-4) + (5R)-5-hydroxy-L-lysine (504-91-6,1190-94-9,3506-26-1,6000-08-4,18899-29-1,18899-30-4,18899-31-5,52153-41-0,78088-29-6,28902-93-4) + (2S)-4-hydroxylysine (15574-69-3) + (2S)-2,6-diamino-3-hydroxyhexanoic acid

Guidance literature:

With oxygen; In water; γ-Irradiation;

DOI:10.1021/tx980118h

upstream raw materials:

(3R,5R,6S)-3-[2-((R)-3-tert-Butoxycarbonyl-2,2-dimethyl-oxazolidin-5-yl)-ethyl]-2-oxo-5,6-diphenyl-morpholine-4-carboxylic acid benzyl ester

(2S,5S)-6-azido-2-benzyloxycarbonylamino-5-hydroxyhexanoic acid

L-lysine

methyl (S)-2-benzyloxycarbonylamino-6-diazo-5-oxohexanoate

Downstream raw materials:

DL-threo-N²,N⁶-bis-(2,4-dinitro-phenyl)-5-hydroxy-lysine lactone

DL-threo-N²,N⁶-bis-(2,4-dinitro-phenyl)-5-hydroxy-lysine

Δ¹-pyrroline-5-carboxylate

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